A method for sulfone conversion via a super electron donor
An electron-donor, electron-based technique for decomposing remaining sulfones and sulfoxides
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Embodiment 1
[0078] Hydrotreated straight-run diesel oil (which contains 500ppmw elemental sulfur, 0.28wt% organic sulfur, and a density of 0.85KG / L) according to figure 2 method of oxidative desulfurization. The reaction conditions are as follows:
[0079] Catalyst: molybdenum-based Mo(VI)
[0080] Response time: 30 minutes
[0081] Temperature: 80°C
[0082] Pressure: 1kg / cm 2
[0083] During the extraction, 93 kg of bis-imidazolidine was used as electron donor. The extraction at 110°C, 1kg / cm 2 pressure and 0.1h -1 LHSV performed.
[0084] The material balances for the oxidation and extraction steps are shown in Tables 1 and 2, respectively. Desulfurized diesel contains 40 ppmw sulfur.
[0085] ODS
[0086] stream name diesel fuel oxidizing agent catalyst catalyst Oxygenated diesel stream type raw material oxidizing agent catalyst waste product flow# unit 111 113 114 117 118 Mutually Oil watery watery watery ...
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