Epoxy composition and epoxy resin molded article
A technology of epoxy composition and epoxy monomer, applied in the field of epoxy composition and epoxy resin molded body, can solve the problems such as unfavorable productivity of epoxy resin molded body, and achieve the effect of excellent thermal conductivity
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Embodiment 1
[0102] Terexylylene-bis-(4-amino-3-methylphenol) diglycidyl ether (DGETAM, epoxy equivalent weight: 228) and 4,4”-dihydroxy-3”-methyl-p- Terphenyl (DHTP-M, hydroxyl equivalent weight: 138) was dissolved in methyl ethyl ketone (MEK) so that the ratio of the number of epoxy groups derived from DGETAM to the number of hydroxyl groups derived from DHTP-M was 1:1, thereby preparing solution, and to the solution was added tetraphenyl tetraphenyl borate , so that its ratio relative to 100 parts by mass of DGETAM is 1 part by mass, thereby preparing the epoxy composition of Example 1.
[0103] The epoxy composition was poured into an aluminum cup and heated to a temperature of about 100°C, whereby the solvent (MEK) was removed to produce a dry solid.
[0104] Then, the dried solid was held in a vacuum chamber at 150° C. for 10 minutes in a state placed on a glass plate, thereby performing melting and defoaming.
[0105] A spacer was placed around the glass plate, and another glass ...
Embodiment 2
[0109] Terexylylene-bis-(4-amino-3-methylphenol) diglycidyl ether (DGETAM, epoxy equivalent weight: 228) and 4,4',4"-methylenol (TrisP -PHBA, hydroxyl equivalent weight: 97) was dissolved in methyl ethyl ketone (MEK) so that the ratio of the number of epoxy groups derived from DGETAM to the number of hydroxyl groups derived from TrisP-PHBA was 1:1 to prepare a solution, and to tetraphenyl borate , so that its ratio relative to 100 parts by mass of DGETAM is 1 part by mass, thereby preparing the epoxy composition of Example 2.
[0110] The epoxy composition was poured into an aluminum cup and heated to a temperature of about 100°C, whereby the solvent (MEK) was removed to produce a dry solid.
[0111] Then, the dried solid was held in a vacuum chamber at 150° C. for 10 minutes in a state placed on a glass plate, thereby performing melting and defoaming.
[0112] A spacer was placed around the glass plate, and another glass plate was further placed thereon, followed by holdin...
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Abstract
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