Multitubular fixed bed reactor and application thereof

A fixed bed reactor and reactor technology, which are applied in chemical instruments and methods, hydrocarbon production from oxygen-containing organic compounds, organic chemistry, etc., can solve the problem of shortened catalyst service life, low reactor load, limited reactor production capacity, etc. problems, to achieve the effect of improving operation flexibility and stability, improving reaction ability, and eliminating reaction hot spots

Inactive Publication Date: 2014-08-20
SHANGHAI RONGYI INVESTMENT MANAGEMENT
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The limitation of the tube-and-tube fixed-bed reactor is that the heat transfer is poor, and hot spots are usually generated, which leads to uneven reaction temperature, shortened service life of the catalyst, and low efficiency; in addition, considering that the reaction fluid passes through the catalyst fixed bed When the pressure drop, the reactor load is...

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  • Multitubular fixed bed reactor and application thereof
  • Multitubular fixed bed reactor and application thereof
  • Multitubular fixed bed reactor and application thereof

Examples

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Embodiment 1

[0057] In this embodiment, the reactor used is a single-tube reactor, where the reaction tubes are as figure 1 As shown, the material of the reaction tube is 302 stainless steel, the cross section is rectangular, the internal dimensions of the formed catalyst chamber are 0.05m in length and 0.02m in width, and the height of the reaction tube is 0.5m.

[0058] The catalyst cavity of the reaction tube is filled with a 10-40 purpose ZSM-5 type MTP catalyst, the catalyst loading is 300g, the raw material is methanol: the methanol aqueous solution with a water mass ratio of 1:1, the raw material inlet temperature is 200 ° C, and the outlet The pressure of the collection chamber is normal pressure, and when the external temperature of the reaction tube is controlled at 460°C, the maximum temperature inside the reaction tube is 470°C, the reactant flow passes through the catalyst bed along the direction perpendicular to the axis of the reactor, and the pressure drop of the bed is <10...

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Abstract

The invention relates to a multitubular fixed bed reactor, which comprises at least one catalyst-loaded reaction tube longitudinally extending along a direction parallel to the axis of the reactor. The height of the reaction tube and the hydraulic diameter of the reaction tube's cross-section are in a ratio of 1-2000, preferably 10-1000, and more preferably 50-500. The reaction tube includes: one or more catalyst chambers, which are used for loading the catalyst to form a catalyst fixed bed; one or more inlet distribution chambers, which are used for leading a reactant flow into the reaction tube and distributing the reactant flow into the catalyst fixed bed; and one or more outlet collection chambers, which are used for collecting the reactant flow and leading the reactant flow out of the reaction tube. Specifically, through arrangement of the inlet distribution chamber(s) and the outlet collection chamber(s), the reactant flow passes through the catalyst fixed bed layer along a horizontal direction perpendicular to the axis of the reactor so as to contact the catalyst and react with the catalyst. The invention also relates to application of the multitubular fixed bed reactor in chemical reactions like endothermic or exothermic reaction.

Description

technical field [0001] The invention relates to a novel tubular fixed-bed reactor and the application of the tubular fixed-bed reactor in chemical reactions such as endothermic or exothermic reactions. Background technique [0002] The tubular fixed-bed reactor is a commonly used reactor in the chemical industry. It is generally used in the process of gas-phase or liquid-phase reactions catalyzed by solid catalysts. The catalyst forms a fixed bed, and the reactant stream passes through the fixed bed to react. [0003] The tubular fixed bed reactor is generally composed of a plurality of reaction tubes connected in parallel, and a catalyst fixed bed is generally arranged in the reaction tube, and the gas and / or liquid reactant flow passes through the catalyst fixed bed along the axial direction of the reaction tube, It contacts with the catalyst and reacts therein, while the heat carrier flows through the reaction tubes for heating or cooling. Therefore, the tubular fixed-be...

Claims

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Application Information

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IPC IPC(8): B01J8/06C07C1/20C07C11/06C07C11/04
CPCY02P30/20Y02P30/40
Inventor 魏小波韩国茹陈伟
Owner SHANGHAI RONGYI INVESTMENT MANAGEMENT
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