Reversibly thermochromic composition
A thermochromic and composition technology, applied in the direction of color-changing fluorescent materials, heat-sensitive coatings, structure changes of writing utensils, etc., can solve the problems of unsmooth writing feeling, difficult to fade, and fading, etc., and achieve the effect of improving visibility
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Embodiment 101~106 and comparative example 101~106
[0270] The compositions of the solid writing materials of Examples and Comparative Examples are shown in the following table. In addition, the numerical value of the composition in a table shows a mass part. In addition, the particle size of the microcapsule pigment was measured with a laser diffraction / scattering type particle size distribution measuring device Model LA-300 (trade name, manufactured by Horiba Seisakusho Co., Ltd.), and the average particle size was calculated on a volume basis based on the value. (median particle diameter) obtained value.
[0271]
[0272] The contents of the raw materials in the table are explained according to the comment numbers.
[0273] (1) Reversible thermochromic microcapsule pigment (T 1 : -16°C, T 2 : -8°C, T 3 : 48°C, T 4 : 58°C, ΔH: 65°C, average particle size: 2.5 μm, reversible thermochromic composition: wall film = 2.6:1.0, color changes from blue to colorless), the heat-fading type reversible thermochromic composition ...
Embodiment 201
[0329] (Production of reversible thermochromic composition)
[0330] Thermochromic Microcapsule A 18 parts by mass
[0331] Myristyl alcohol (endothermic phase transition compound) 20 parts by mass
[0332] 32 parts by mass of ion-exchanged water
[0333] Stir the above mixture with a magnetic stirrer until uniform. The obtained mixture was dried at room temperature, whereby a reversible thermochromic composition 201 was obtained.
Embodiment 202~211
[0335] A reversible thermochromic composition was obtained in the same manner as in Example 201, except that the thermochromic microcapsules and endothermic microcapsules shown in Table 4 were used instead of the thermochromic microcapsules A and myristyl alcohol.
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