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Coal tar ingredient analysis instrument

A component analysis and coal tar technology, applied in the field of coal tar component analyzer, can solve the problems of difficult to guarantee the accuracy of measurement results, low accuracy of manual observation test, cumbersome process and time cost, etc., to improve test accuracy, reduce operation difficulty, The effect of ensuring accuracy

Inactive Publication Date: 2014-09-03
LIAONING WANHONG LASER TECH
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  • Summary
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the process of determining the distillation range of artificial distillation, the experimental operators use the naked eye to observe and record key parameters such as the initial boiling point, final boiling point, and dry point in the distillation range. The distillation range curve is also calculated and drawn manually. Due to the low accuracy of manual observation , slow speed, and many human-influenced factors make it difficult to guarantee the accuracy of the measurement results
For this reason, some large coking enterprises also conduct gas chromatographic analysis to determine the product composition structure, and the drawing of their distillation curves mostly adopts the method of establishing mathematical models, or uses the multiple regression method to establish the chromatographic curve of the distillation range of benzene, because These measurement processes are obtained by means of simulation, and there is still a certain gap from the real results. Therefore, it takes a long time of experience accumulation to achieve precise control of the determination of the distillation range of one of the media. If you want to master dozens of The law of determination of the distillation range of coking substances, the complicated process and the time cost can be imagined

Method used

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Examples

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Embodiment 1

[0049] [Example 1] Apply the coal tar component analyzer of the present invention to measure the content of 5 components in a coal tar product, and draw the distillation range curve, the 5 components are respectively: benzene, toluene, ethylbenzene , p-xylene, meta-xylene and ortho-xylene.

[0050] This embodiment is carried out according to the method for determining the distillation curve curve of the present invention. During the experiment, the temperature of the heating furnace 9 is controlled so that the sample in the distillation bottle 1 is heated up at a rate of 6 ° C / min. After the distillate is distilled , control the heating temperature so that the droplet temperature is controlled at 20°C, the computer automatically counts the distillation range data, and the content inspection report of each component is as follows:

[0051] Content inspection report of each component

[0052]

[0053] The distillation range curve figure of the present embodiment is shown i...

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Abstract

The invention relates to a coal tar ingredient analysis instrument. The coal tar ingredient analysis instrument comprises a distilling flask, a flow diversion pipe, a condensing pipe, a liquid collecting flask, and a sample weighing device, a lifting support frame, a heating furnace, a distillate weighing device and a circulating water device which are connected with a control system. By precisely and automatically controlling a whole distillation process by virtue of the coal tar ingredient analysis instrument, the measuring accuracy of the distillate quantity of a corresponding substance can reach a distilling temperature interval of 0.1 DEG C, and the distillate quantity of each ingredient is recorded in a distilling range curve manner. Compared with the prior art, the coal tar ingredient analysis instrument has the beneficial effects that the automation of a coal tar distilling experiment is realized, the measuring accuracy is improved, and the accuracy of a measuring result is guaranteed; a distilling range curve graph is automatically generated; various complex ingredients in coal tar can be finely distinguished, the boiling temperature of each ingredient can be measured, and the mass percentage of each ingredient in coal tar can be accurately and quantitatively calculated; the operation difficulty and the labor intensity of an experimenter are reduced; the application prospect of the instrument is wide.

Description

technical field [0001] The invention relates to the technical field of coal tar distillation range analysis, in particular to a coal tar component analyzer. Background technique [0002] In order to accurately understand the actual content of different substances in coal tar, and at what temperature they can be separated and used, so as to adjust the control conditions in production according to the actual situation, it is necessary to conduct detailed analysis through coal tar distillation experiments. During the experiment, precise temperature control is very important. [0003] The distillation range analysis of coal tar includes the determination of the composition structure, the content of each component and the distillation range. At present, most of the analysis and determination work is still done manually by chemical analysis and distillation. Coal tar products have thousands of distillate substances during the distillation process, of which only dozens of varietie...

Claims

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Application Information

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IPC IPC(8): G01N5/04
Inventor 王姝杨亚明李瑾王辉
Owner LIAONING WANHONG LASER TECH
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