Method for accurately measuring shale porosity by adopting low-field nuclear magnetic resonance
A low-field nuclear magnetic resonance and shale porosity technology, which is applied in the field of detection and mining, can solve the problems of poor contrast and large difference in helium porosity, and achieve the effect of improving accuracy and precision and convenient operation.
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[0045] Such as Figure 1-Figure 9 The method for accurately measuring shale porosity by using low-field nuclear magnetic resonance includes measuring shale porosity by low-field nuclear magnetic resonance technology, and calibrating by helium porosity, so as to obtain the shale porosity measured by nuclear magnetic resonance Reasonable parameters for accurate determination.
[0046] figure 1 In order to accurately measure the porosity of shale by low-field nuclear magnetic resonance, the steps are as follows:
[0047] 1) Make a standard sample and establish a marking equation: a small amount of CuSO 4 ·5H 2 O is fully dissolved in an appropriate amount of distilled water, so that CuSO 4 Solution transverse relaxation time (T 2 ) between 10 and 100ms; use a digital titrator to take a certain mass interval of CuSO 4 solution into the standard sample bottle; the standard sample is placed in multiple groups of different echo times and waiting times, that is, in the NMR instr...
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