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Protection method of quartz tube

A quartz tube and sacrificial layer technology, applied in chemical instruments and methods, gaseous chemical plating, crystal growth, etc., can solve the problem of increasing the peeling off of the quartz tube 110 polysilicon film, affecting the reliability of the low-pressure chemical vapor deposition process, and increasing the low-pressure chemical vapor deposition process. Problems such as deposition equipment, to achieve good stretchability and porosity, relieve stress release, and prevent particles from falling off

Active Publication Date: 2017-05-24
SEMICON MFG INT (SHANGHAI) CORP
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Problems solved by technology

The presence of the stress stripes not only reduces the number of times the quartz tube 110 is used, but also increases the probability of peeling off the polysilicon film on the quartz tube 110 during the process of depositing the polysilicon film, thereby increasing the low pressure chemical vapor deposition equipment 100. High risk of particles that affect the reliability of the low pressure chemical vapor deposition process

Method used

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  • Protection method of quartz tube
  • Protection method of quartz tube
  • Protection method of quartz tube

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Embodiment Construction

[0030] In the low-pressure chemical vapor deposition equipment of the prior art, when the process of low-pressure chemical vapor deposition is carried out, many stress stripes will appear on the inner wall of the quartz tube, and the deposited film will be deposited on the inner wall of the quartz tube. Existence causes the deposited film to peel off to form particles. After in-depth research on the existing low-pressure chemical vapor deposition equipment, the inventor found that the material of the wafer is silicon, and the material of the quartz tube is silicon oxide. However, the thermal expansion coefficient of silicon is 2.6×10 - 6 K -1 , the thermal expansion coefficient of silicon oxide is 0.5×10 -6 K -1 , due to the large difference in thermal expansion coefficient between silicon and silicon oxide, when the low-pressure chemical vapor deposition process is performed, the temperature in the low-pressure chemical vapor deposition equipment is the temperature suitabl...

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Abstract

The invention discloses a quartz tube protection method. The method comprises the following steps: providing a quartz tube; carrying out primary pickling on the inner wall of the quartz tube to make the inner wall of the quartz tube have a rough surface; preparing a sacrificial layer on the rough surface of the inner wall of the quartz tube; carrying out secondary pickling on the inner wall of the quartz tube to remove the sacrificial layer; and preparing a buffer layer on the inner wall of the quartz tube. In the quartz tube protection method, the sacrificial layer can fill the rough surface of the inner wall of the quartz tube and can effectively alleviate the release of the stress of a deposited film in order to reduce or eliminate stress fringes on the inner wall of the quartz tube; and the outermost side of the inner wall of the quartz tube is provided with the buffer layer, and the buffer layer can well adsorb the deposited film and prevent the shredding of particles to reduce the particles of a low pressure chemical vapor deposition apparatus in order to improve the reliability of a low pressure chemical vapor deposition technology.

Description

technical field [0001] The invention relates to the technical field of semiconductor manufacturing, in particular to a protection method for a quartz tube. Background technique [0002] LPCVD (low pressure chemical vapor deposition), Chinese for low-pressure chemical vapor deposition, is one of the main processes in the field of large-scale integration (LSI) and very large-scale integration (VLSI) and semiconductor optoelectronic device technology. LPCVD technology can improve the quality of deposited thin films, so that the film layer has the advantages of good uniformity, low defect density, and good step coverage. It has become the main method for preparing thin films such as polycrystalline silicon, single crystal silicon, and silicon nitride. [0003] Low-pressure chemical vapor deposition equipment in the prior art is generally a quartz tube furnace, such as figure 1 As shown, the low pressure chemical vapor deposition equipment 100 includes a quartz tube 110 , a sili...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C16/44C30B25/08
Inventor 沈建飞
Owner SEMICON MFG INT (SHANGHAI) CORP
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