Gear wear-resisting lubricating grease composition and preparation method thereof
A technology for lubricating grease composition and gears, applied in lubricating compositions, petroleum industry, etc., can solve the problems of gear damage, high cost, complicated preparation process, etc., and achieve the effect of improving friction performance and prolonging service life
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Embodiment 1
[0025] Raw materials: perfluoropolyether oil 70kg, polytetrafluoroethylene 5kg (particle size 0.5μm), antioxidant 1010 2kg, oxidized paraffin 1kg, carbon black 2kg, tungsten disulfide 1kg (particle size 3μm).
[0026] (1) Add 42kg of perfluoropolyether oil and 5kg of polytetrafluoroethylene into the stirred reactor, raise the temperature to 100°C, and stir for 2 hours;
[0027] (2) Add the remaining perfluoropolyether oil, cool down to 70°C and stir at constant temperature for 1 hour, then add 2kg of antioxidant 1010, 1kg of oxidized paraffin, 2kg of carbon black and 1kg of tungsten disulfide after cooling down to 40°C, and stir evenly take out;
[0028] (3) Apply the product of step 2 taken out on a clean aluminum plate, put it in an oven and bake it at 200°C for 4 hours, then cool to room temperature, add it to a three-roller machine, grind it three times, and then degas it in a vacuum degasser to obtain Anti-wear grease composition for gears.
[0029] The performance test...
Embodiment 2
[0031] Raw materials: perfluoropolyether oil 90kg, polytetrafluoroethylene 20kg (particle size 0.1μm), antioxidant 168 5kg, benzotriazole 5kg, carbon black 6kg, tungsten disulfide 5kg (particle size 100μm).
[0032] (1) Add 54kg of perfluoropolyether oil and 20kg of polytetrafluoroethylene into the stirred reactor, raise the temperature to 120°C, and stir for 2 hours;
[0033] (2) Add the remaining perfluoropolyether oil, cool to 70°C and stir at constant temperature for 1 hour, then add 5kg of antioxidant 168, 5kg of benzotriazole, 6kg of carbon black, kg of tungsten disulfide 5, Take out after stirring well;
[0034] (3) Apply the product of step 2 taken out on a clean aluminum plate, put it in an oven and bake it at 200°C for 4 hours, then cool to room temperature, add it to a three-roller machine, grind it three times, and then degas it in a vacuum degasser to obtain Anti-wear grease composition for gears.
[0035] The performance test results of the prepared grease are ...
Embodiment 3
[0037] Raw materials: perfluoropolyether oil 80kg, polytetrafluoroethylene 10kg (particle size 0.8μm), antioxidant 1010 3kg, benzotriazole 2kg, carbon black 4kg, tungsten disulfide 3kg (particle size 50μm).
[0038] (1) Add 48kg of perfluoropolyether oil and 10kg of polytetrafluoroethylene into the stirred reactor, raise the temperature to 110°C, and stir for 2 hours;
[0039] (2) Add the remaining perfluoropolyether oil, cool down to 70°C and stir for 1 hour at a constant temperature, then add 3kg of antioxidant 1010, 2kg of benzotriazole, 4kg of carbon black, 3kg of tungsten disulfide, and stir Take out after uniform;
[0040] (3) Apply the product of step 2 taken out on a clean aluminum plate, put it in an oven and bake it at 200°C for 4 hours, then cool to room temperature, add it to a three-roller machine, grind it three times, and then degas it in a vacuum degasser to obtain Anti-wear grease composition for gears.
[0041] The performance test results of the prepared g...
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