Hyper-gravity reactor and reaction method

A hypergravity reactor and reaction technology, applied in chemical instruments and methods, chemical methods for reacting liquids and gaseous media, chemical/physical/physical-chemical mobile reactors, etc., to achieve low requirements for mutual solubility and widening The effect of the scope of application

Active Publication Date: 2015-02-25
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The invention improves the structure and layout of the liquid feed port and the spray pipe of the supergravity reactor, so that the mixing of the liquid catalyst and the liquid reactant or the two liquid reaction materia

Method used

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  • Hyper-gravity reactor and reaction method
  • Hyper-gravity reactor and reaction method

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Embodiment

[0034] like figure 1 , figure 2 , image 3 Shown, a supergravity reactor. The high-gravity reactor 11 is provided with two liquid feed ports 1, and the two liquid feed ports 1 are respectively connected to respective liquid distributors, and the spray pipes 5 of the two liquid distributors are independent and arranged on a rotating bed On the concentric ring with the central axis as the center of the circle, the number of spray pipes of the two liquid distributors is the same and arranged at intervals in sequence.

[0035] Catalyst preparation: This catalyst uses a 1:1 mixture of nitric acid and hydrochloric acid to dissolve metal Pd, control the dissolved Pd particle size within the range of 5-50nm, and then use NaOH solution to adjust the pH value of the solution between 6.5-7, and finally Add deionized water to make aqueous catalyst. The active component Pd is evenly suspended (similarly dissolved) in the whole solution in the state of nanoparticles. During the prepara...

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Abstract

The invention discloses a hyper-gravity reactor and a reaction method. The hyper-gravity reactor is provided with two liquid inlets. Two liquid inlets are respectively connected to responding liquid distributors. The spraying pipes of two liquid distributors are separated and arranged on concentric rings, which take the middle shaft of a rotation bed as the center. The reaction method comprises the following steps: feeding a reaction material and a catalyst or two reaction materials into the hyper-gravity reactor from the two liquid inlets, then spraying the reaction material and the catalyst or two reaction materials on the internal edges of rotating filling materials or solid catalysts from two individual spraying pipes so as to mix the reaction material and the catalyst or two reaction materials, carrying out reactions by contacting the reaction material and the catalyst or two reaction materials, or carrying out reactions by contacting the mixture with gas. The structure and distribution of the liquid inlets and spraying pipes of the hyper-gravity reactor are both improved so as to mix the liquid catalyst and liquid reactant in a hyper-gravity field, because the mixing effect is good in a hyper-gravity field. At the same time the problems of the post treatment for separating the liquid catalyst and the liquid products are also solved and simplified.

Description

technical field [0001] The invention relates to the field of reaction engineering, and more specifically, relates to a high-gravity reactor and a reaction method. Background technique [0002] Catalytic reactions are ubiquitous in petrochemical, chemical industry, bioengineering, environmental protection and other fields. Catalytic reactions are carried out in various reactors such as fixed beds and fluidized beds. Reactors provide reaction materials, reaction materials and homogeneous Or the physical space where heterogeneous catalysts come into contact. The selection of the reactor often determines the reaction materials, and the contact mode between the reaction materials and the catalyst is very important to the catalytic reaction efficiency. [0003] Hypergravity technology is an engineering technology developed in the 1970s. The EP0023745A3 patent of the British Imperial Chemical Company (ICI) involves the research on the chemical separation unit operation----distillat...

Claims

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Application Information

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IPC IPC(8): B01J19/28B01J10/00C07C5/03C07C9/10
CPCY02P20/584B01J8/10B01J8/085C07C5/03C07C9/10
Inventor 李文铭李振虎郝国均张文胜曾东
Owner CHINA PETROLEUM & CHEM CORP
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