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A kind of preparation method of water-soluble polymer surface graft modification machine-made sand

A technology of surface graft modification and water-soluble polymer, which is applied in the field of preparation of water-soluble polymer modified machine-made sand, can solve the problems of increasing the flow resistance of the mixture, increasing the water demand, increasing the cost, etc., and achieving Improve the flexural strength, improve the ease of use, and reduce the cost of use

Inactive Publication Date: 2016-08-31
HEFEI UNIV OF TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, with the rapid development of the construction industry, the demand for natural sand in construction projects is increasing day by day. However, as a local resource, natural sand cannot be regenerated in a short period of time. The existing natural sand can no longer meet the needs of engineering construction. , so the use of machine-made sand to prepare concrete has become an inevitable trend in future development
[0003] The roughness of natural sand is relatively small, the surface is smooth, and the grain shape is relatively round, while the roughness of machine-made sand is relatively large, which will increase the flow resistance of the mixture, increase the water demand, and also cause the water retention of freshly mixed concrete. Poor cohesion, easy segregation, bleeding, difficult to meet the requirements of the preparation of high-performance concrete
According to the principle of close packing, fine aggregates with small porosity need less cementitious materials when making concrete, while the particles of machine-made sand are sharper and have larger porosity. more, this will inevitably increase the cost

Method used

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  • A kind of preparation method of water-soluble polymer surface graft modification machine-made sand
  • A kind of preparation method of water-soluble polymer surface graft modification machine-made sand
  • A kind of preparation method of water-soluble polymer surface graft modification machine-made sand

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Embodiment 1

[0027] In this example, the water-soluble surface graft modified machine-made sand is prepared according to the following steps:

[0028] Step 1: Hydroxylation treatment:

[0029] First, in an ice-water bath, slowly add 10 mL of hydrogen peroxide with a mass concentration of 30% into 50 mL of concentrated sulfuric acid with a mass concentration of 98%, and stir while adding to obtain a Piranha solution;

[0030] Then the Piranha solution was added to a beaker equipped with 30 g of machine-made sand, and reacted slightly at 80° C. in a water bath for 4 h to obtain reaction solution A. The Piranha solution in the reaction solution A was removed by centrifugation, and the resulting solid product was washed with deionized water for more times, and finally vacuum-dried to obtain hydroxylated machine-made sand;

[0031] Step 2: Coupling agent modification

[0032] Add 10 g of the hydroxylated machine-made sand obtained in step 1 and coupling agent KH-5707 mL into toluene as a solv...

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Abstract

The invention discloses a preparation method of water-soluble macromolecular surface-grafted modified machine-made sand. The method is characterized by comprising steps as follows: firstly, performing hydroxylation treatment on machine-made sand to obtain hydroxylated machine-made sand, then modifying the hydroxylated machine-made sand with a coupling agent to obtain a coupling-agent-modified machine-made sand, and enabling the coupling-agent-modified machine-made sand, acrylic acid and methyl allyl polyethenoxy ether to be subjected to grafting polymerization through a grafting polymerization reaction to obtain the water-soluble macromolecular surface-grafted modified machine-made sand. The water-soluble macromolecular surface-grafted modified machine-made sand can effectively enhance the workability and the breaking strength of machine-made sand concrete and can be widely applied to building fields of bridges, roads, railways and the like.

Description

1. Technical field: [0001] The invention relates to a preparation method of water-soluble polymer modified machine-made sand. 2. Background technology [0002] For a long time, natural sand has been widely used as fine aggregate for concrete preparation. However, with the rapid development of the construction industry, the demand for natural sand in construction projects is increasing day by day. However, as a local resource, natural sand cannot be regenerated in a short time. The existing natural sand can no longer meet the needs of engineering construction. , so the use of machine-made sand to prepare concrete has become an inevitable trend in future development. [0003] The roughness of natural sand is relatively small, the surface is smooth, and the grain shape is relatively round, while the roughness of machine-made sand is relatively large, which will increase the flow resistance of the mixture, increase the water demand, and also cause the water retention of freshly...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B14/06
Inventor 王文平李国庆吕晓勇李小龙
Owner HEFEI UNIV OF TECH
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