Industrial production method for simultaneously extracting tea seed oil and tea saponin
A production method and tea saponin technology, which are applied in the directions of fat oil/fat production, chemical instruments and methods, sugar derivatives, etc., can solve the problems of long production cycle, increase production cost, increase the difficulty of extracting tea seed oil, etc. The effect of improving product extraction rate, improving product quality, and broadening the scope of application
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Embodiment 1
[0021] After the cleaned camellia seeds are softened at 45°C for 30 minutes, the kernels and shells are crushed into 5-8 petals by a pulverizer, and the crushed particles are passed through a shell-kernel separation sieve to effectively separate the shells from the kernels. The kernels contain 3wt% shells ; The separated Camellia oleifera seeds are extruded at a low temperature of 85°C and sent to the extraction equipment.
[0022] Camellia oleifera seeds were extracted with a homogeneous mixed solvent of ether and alcohol, the extraction temperature was 52°C, and the extraction time was 130 minutes to obtain a homogeneous mixed solvent extract containing camellia oil and tea saponin and camellia seed meal; after extraction of camellia seed kernels, 65 ℃ drying and precipitating to obtain Camellia oleifera seed meal.
[0023] The ether in the homogeneous mixed solvent of ether and alcohol is diethyl ether; the alcohol is methanol; the ether solvent in the homogeneous mixed sol...
Embodiment 2
[0028] After the cleaned camellia seeds are softened at a low temperature of 55°C for 20 minutes, the kernels and shells are crushed into 5-8 petals by a pulverizer, and the crushed particles are passed through a shell-kernel separation sieve to effectively separate the shells from the kernels. The kernels contain 4.5wt shells %; The separated Camellia oleifera seeds are extruded at a low temperature of 82°C and sent to the extraction equipment.
[0029] Camellia oleifera seeds were extracted with a homogeneous mixed solvent of ether and alcohol, the extraction temperature was 55°C, and the extraction time was 160 minutes to obtain a homogeneous mixed solvent extract containing camellia oil and tea saponin, as well as camellia seed meal; after extraction, 75 ℃ drying and precipitating to obtain Camellia oleifera seed meal.
[0030] The ether in the homogeneous mixed solvent of ether and alcohol is isopropyl ether; the alcohol is a mixture of ethanol and isopropanol at a volume...
Embodiment 3
[0035]After the cleaned camellia seeds are softened at 48°C for 23 minutes, the kernels and shells are crushed into 5-8 pieces of granules by a pulverizer, and the crushed granules are passed through a shell-kernel separation sieve to effectively separate the shells from the kernels. The shells in the kernels are less than 4wt %; The separated Camellia oleifera seeds are extruded at a low temperature of 83°C and sent to the extraction equipment.
[0036] Camellia oleifera seeds were extracted with a homogeneous mixed solvent of ether and alcohol, the extraction temperature was 59°C, and the extraction time was 180 minutes to obtain a homogeneous mixed solvent extract containing camellia oil and tea saponin and camellia seed meal; after extraction of camellia seed kernels, 80 ℃ drying and precipitating to obtain Camellia oleifera seed meal.
[0037] The ether in the homogeneous mixed solvent of ether and alcohol is diethyl ether; the alcohol is isopropanol; and the ether solven...
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