Three-dimensional structure graphene composite intermediate layer assisted brazing method

A technology of graphene composite and three-dimensional structure, which is applied in the direction of coating, welding equipment, metal material coating process, etc., can solve the problems of poor mechanical properties of brazed joints such as joint residual stress, improve dispersion, avoid agglomeration, repeat strong effect

Active Publication Date: 2017-01-04
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The present invention aims to solve the problem of poor mechanical properties of brazed joints due to the fact that the joints are prone to produce large residual stresses during the existing brazing process, and provides a method for assisting brazing with a three-dimensional graphene composite intermediate layer

Method used

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  • Three-dimensional structure graphene composite intermediate layer assisted brazing method

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specific Embodiment approach 1

[0019] Specific embodiment one: the method for assisted brazing of the three-dimensional structure graphene composite intermediate layer described in the present embodiment is specifically carried out according to the following steps:

[0020] 1. Ultrasonic pretreatment of the metal foam with acetone for 10 to 20 minutes to obtain a metal foam with impurities removed from the surface;

[0021] The metal foam is Ni foam or Cu foam;

[0022] 2. Put the metal foam from which impurities have been removed from the surface in a chemical vapor deposition device, evacuate until the pressure is below 20Pa, pass in argon gas, adjust the flow rate of argon gas to 10sccm~50sccm, and adjust the pressure in the chemical vapor deposition device to 50Pa~ 300Pa, and under the pressure of 50Pa~300Pa and argon atmosphere, the temperature is raised to 800℃~1200℃;

[0023] 3. Feed methane, adjust the gas flow rate of methane to 5 sccm to 40 sccm, adjust the gas flow rate of argon to 60 sccm to 95...

specific Embodiment approach 2

[0034] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the material to be welded described in step 4 is a metal material or ceramic material; the described material to be welded is polished with sandpaper, and then ultrasonically pretreated in acetone 5min~10min. Others are the same as in the first embodiment.

specific Embodiment approach 3

[0035] Embodiment 3: This embodiment differs from Embodiment 1 or Embodiment 2 in that the brazing filler metal described in Step 4 is AgCuTi brazing filler metal or TiNi brazing filler metal. Others are the same as in the first or second embodiment.

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Abstract

The invention relates to the field of material welding, in particular to an auxiliary brazing method for a grapheme composite middle layer of a three-dimensional structure. The problem that in the existing brazing process, a connector is prone to generating large residual stress to lead to the poor mechanical property of the brazing connector is solved. The method includes the steps that impurities on the surface of foam metal are removed, the foam metal is placed in a chemical vapor deposition device, argon is injected into the device, the gas flow and pressure are adjusted, then temperature is made to rise, methane is injected, the gas flow and pressure are adjusted to carry out deposition, and the grapheme composite middle layer of the three-dimensional structure is obtained after deposition is completed; the grapheme composite middle layer of the three-dimensional structure is placed between two materials to be welded, brazing filler metal is placed between faces to be welded, the combination is placed in a vacuum brazing furnace, the vacuum brazing furnace is vacuumized, the heat is preserved at high temperature, and then the vacuum brazing furnace is cooled to complete the auxiliary brazing process of the grapheme composite middle layer of the three-dimensional structure. The method is used for auxiliary brazing for the grapheme composite middle layer of the three-dimensional structure.

Description

technical field [0001] The invention relates to the field of material welding. Background technique [0002] The following two major problems are mainly faced in the brazing process of materials. First of all, there is a large difference in thermal expansion coefficient between materials, and the joints are prone to generate large residual stress during the brazing process. Residual stress will seriously weaken the mechanical properties of joints, and even cause damage to already connected joints. At present, the residual stress of the joint can be relieved and the performance of the brazed joint can be improved by optimizing the solder and adjusting the structure of the brazing intermediate layer. Secondly, the wetting of the surface of different materials and solder is quite different, resulting in problems such as insufficient interfacial reaction and discontinuous reaction layer, which will have a serious impact on the performance of the joint. Graphene, usually refer...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B23K1/008B23K1/20C23C16/26
CPCB23K1/008B23K1/20C23C16/26
Inventor 亓钧雷林景煌罗大林张天琪谈雪琪冯吉才
Owner HARBIN INST OF TECH
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