Detection method for effective components in silky fowl tablet

A detection method and technology of active ingredients, applied in the medical field, can solve problems such as waste, large amount of water, and inability to separate

Inactive Publication Date: 2015-07-01
津药达仁堂集团股份有限公司乐仁堂制药厂
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0011] Volatile oil is a unique component in traditional Chinese medicine, which has a variety of pharmacological effects: traditional steam distillation was used for volatile oil in the past. The amount of water is large and cannot be separated, so it is finally discarded, resulting in waste; in addition, the volatile oil components of some traditional Chinese medicines are soluble in water and do not form an oil-water separation layer, so they cannot be separated

Method used

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  • Detection method for effective components in silky fowl tablet
  • Detection method for effective components in silky fowl tablet

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] 5-10g black-bone chicken, 108g antler glue, 54g vinegar turtle shell, 40g calcined oyster, 40g mulberry octopus, 108g ginseng, 27g astragalus, 122g angelica, 108g white peony root, 108g vinegar cyperus, 54g asparagus, 27g licorice, 215g rehmannia glutinosa , Rehmannia glutinosa 216g, Chuanxiong 54g, Yin Bupleurum 22g, Salvia miltiorrhiza 108g, Chinese yam 108g, Gorgon 54g, antler cream 40g.

[0044] The above 20 flavors, yam and antler gum are crushed into fine powder, Cyperus cyperus extracts volatile oil, black-bone chicken is cut into small pieces, add water and cook for 1 hour, add an appropriate amount of solid paraffin while it is hot, stir to melt, let stand, discard The upper layer of wax and fat is solid, the decoction is stirred into a homogenate, an appropriate amount of papain is added, stirred, hydrolyzed for 5 hours, boiled for 5 minutes, centrifuged, the supernatant is taken, concentrated under reduced pressure to form a thick paste, and dried under reduce...

Embodiment 2

[0047] Black-bone chicken 5g, deer horn glue 100g, vinegar turtle 50g, calcined oyster 30g, mulberry octopus 50g, ginseng 100g, astragalus 20g, angelica 120g, white peony root 100g, vinegar Cyperus 100g, asparagus 50g, licorice 20g, rehmannia glutinosa 200g, rehmannia glutinosa Yellow 200g, Chuanxiong 50g, Yinbupleurum 20g, Salvia miltiorrhiza 100g, Chinese yam 100g, Gorgon 50g, Deer horn cream 30g.

Embodiment 3

[0049] 15g black-bone chicken, 110g antler glue, 60g vinegar turtle shell, 50g calcined oyster, 60g mulberry octopus, 110g ginseng, 30g astragalus, 130g angelica, 110g white peony, 110g vinegar cyperus, 60g asparagus, 30g licorice, 220g rehmannia glutinosa, rehmannia glutinosa Huang 220g, Chuanxiong 60g, Yin Bupleurum 30g, Salvia miltiorrhiza 110g, Chinese yam 110g, Euryale 60g, Deer horn cream 50g.

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Abstract

The invention relates to a detection method for effective components in a silky fowl tablet. The method includes the steps of: (1) quantitative detection of paeoniflorin and liquiritin; and (2) qualitative detection of Cyperus rotundus, paeoniflorin and liquiritin. The method has good specificity and high sensitivity, and can reliably detect the end product quality, thus being suitable for industrial routine inspection.

Description

technical field [0001] The invention relates to the medical field, in particular to a detection method for active ingredients of traditional Chinese medicines. Background technique [0002] Black-bone Chicken Baifeng Tablets are composed of black-bone chicken, ginseng, white peony root, salvia miltiorrhiza, angelica, cyperus and other 20 traditional Chinese medicines. It has the effect of nourishing qi and blood, regulating menstruation and stopping belt. . Studies have shown that Wuji Baifeng Tablets can reduce triglycerides and oxidized low-density lipoproteins in rats, prevent arteriosclerosis, prevent osteoporosis, and protect the liver. It has potential medicinal value for Alzheimer's disease. Therefore, the clinical application of Wuji Baifeng Tablets is becoming wider and wider, and there are more and more domestic manufacturers currently producing it. In order to control the quality of Wuji Baifeng Tablets, the 2005 Pharmacopoeia also has content determination meth...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90
Inventor 王磊金兆祥王琳张宇
Owner 津药达仁堂集团股份有限公司乐仁堂制药厂
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