Atomic force microscope scanning thermal probe and preparation method thereof

A technology of atomic force microscopy and scanning heat, applied in scanning probe technology, scanning probe microscopy, measuring devices, etc., can solve problems such as low accuracy, large error, and decreased spatial resolution, so as to prevent corrosion , reduce errors, improve accuracy and spatial resolution

Active Publication Date: 2015-07-08
SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the existing scanning thermal probe of the atomic force microscope has the problem of large error and low accuracy when measuring the thermal properties of the sample.
When there is a water film on the contact surface between the probe and the sample, the error is greater, and the spatial resolution of the test is also severely reduced

Method used

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  • Atomic force microscope scanning thermal probe and preparation method thereof
  • Atomic force microscope scanning thermal probe and preparation method thereof
  • Atomic force microscope scanning thermal probe and preparation method thereof

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Embodiment Construction

[0019] The present invention will be described in further detail below in combination with specific embodiments and with reference to the accompanying drawings.

[0020] The present invention analyzes the source of error during probe detection, part of the heat emitted by the probe is absorbed by the surface of the sample through the heat conduction between the probe and the sample, part of it enters the air around the probe tip, and part of it is conducted through the cantilever. release, which makes the determination of the part of the heat absorbed by the sample, such as directly equivalent to the heat released by the probe tip as the heat absorbed by the sample, there is a large error. In view of the above analysis, it can be seen that the accuracy of probe detection is closely related to the heat conduction between the probe and the sample. From the perspective of improving the heat conduction of the probe, the present invention improves the structure of the probe tip and ...

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Abstract

The invention discloses an atomic force microscope scanning thermal probe and a preparation method thereof. The obtained atomic force microscope scanning thermal probe comprises a probe cantilever, a probe tip, a graphene thin film layer and a low thermal conductivity layer, and the thermal conductivity of the low thermal conductivity layer ranges from 0.2 W/mK to 2 W/mK; the probe tip is located at one end of the probe cantilever, and the probe tip is coated with the graphene thin film layer which is coated with the low thermal conductivity layer, only the portion, corresponding to a probe tip body, of the graphene thin film layer is coated with the low thermal conductivity layer, and the portion, corresponding to the point of the probe tip, of the graphene thin film layer is not coated with the low thermal conductivity layer. By means of the atomic force microscope scanning thermal probe and the preparation method thereof, the accuracy and the resolution ratio of atomic force microscope thermal tests can be improved.

Description

【Technical field】 [0001] The invention relates to the field of atomic force microscopes, in particular to an atomic force microscope scanning thermal probe and a preparation method thereof. 【Background technique】 [0002] The atomic force microscope uses the interaction force between atoms and molecules to accurately image the surface topography of the material. When the probe tip approaches the sample surface, the interaction force between the two causes the cantilever to bend. The four-quadrant photodetector is used to detect the bending , the magnitude of the force can be calculated using Hooke's law, and the surface morphology of the sample can be inferred from the force the probe bears at different scanning points. Since its invention in 1986, from the initial morphological characterization to the current mechanical, electrical, magnetic, and thermal characterization, the functions have been quite complete, and have been used in many disciplines such as physics, chemist...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01Q60/38
Inventor 杜鸿达姚光锐郑心纬李佳干林褚晓东康飞宇李宝华杨全红徐成俊贺艳兵
Owner SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV
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