A kind of production method of dry-mixed mortar additive
A production method and technology for dry-mixed mortar, which are applied in separation methods, chemical instruments and methods, distillation and separation, etc., can solve problems such as difficult control, high equipment investment, and complex process.
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Embodiment 1
[0119] Embodiment 1: the production of dry mix mortar additive
[0120] The implementation steps of this embodiment are as follows:
[0121] A. Hydrolysis reaction
[0122] Allow the distillation residue discharge that produces when producing dichloropropanol by the glycerin method to be sent in the hydrolysis reactor 3 through the first pump 1 by the pipeline, allow the 15% hydrochloric acid aqueous solution by weight to be sent by the pipeline through the second pump 2 simultaneously In the hydrolysis reaction kettle 3, the distillation residue discharge and the hydrochloric acid aqueous solution were subjected to a hydrolysis reaction for 12 hours at a temperature of 116° C. under normal pressure and stirring conditions according to their weight ratio of 1:0.52, to obtain a hydrolysis reaction material;
[0123] The hydrolysis reaction system composed of distillation residue effluent and hydrochloric acid aqueous solution is also undergoing a vaporization process while und...
Embodiment 2
[0138] Embodiment 2: the production of dry mix mortar additive
[0139] The implementation steps of this embodiment are as follows:
[0140] A. Hydrolysis reaction
[0141] Allow the distillation residue discharge that produces when producing dichloropropanol by the glycerin method to be sent in the hydrolysis reactor 3 through the first pump 1 by the pipeline, allow the 15% hydrochloric acid aqueous solution by weight to be sent by the pipeline through the second pump 2 simultaneously In the hydrolysis reaction kettle 3, the distillation residue discharge and the hydrochloric acid aqueous solution are subjected to a hydrolysis reaction for 10 hours at a temperature of 112° C., under normal pressure and stirring conditions according to their weight ratio of 1:0.55, to obtain a hydrolysis reaction material;
[0142] The hydrolysis reaction system composed of distillation residue effluent and hydrochloric acid aqueous solution is also undergoing a vaporization process while und...
Embodiment 3
[0157] Embodiment 3: the production of dry mix mortar additive
[0158] The implementation steps of this embodiment are as follows:
[0159] A. Hydrolysis reaction
[0160] Allow the distillation residue discharge that produces when producing dichloropropanol by the glycerin method to be sent in the hydrolysis reactor 3 through the first pump 1 by the pipeline, allow the 15% hydrochloric acid aqueous solution by weight to be sent by the pipeline through the second pump 2 simultaneously In the hydrolysis reaction kettle 3, the distillation residue discharge and the hydrochloric acid aqueous solution are subjected to a hydrolysis reaction for 8 hours at a temperature of 110° C. under normal pressure and stirring conditions according to their weight ratio of 1:0.6, to obtain a hydrolysis reaction material;
[0161] The hydrolysis reaction system composed of distillation residue effluent and hydrochloric acid aqueous solution is also undergoing a vaporization process while underg...
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