Method for improving resistance of martensite heat-resistant steel to liquid metal corrosion
A liquid metal and heat-resistant steel technology, applied in the field of metal surface treatment, can solve the problems of restricting the sustainable development of nuclear power and poor wettability, and achieve the effect of improving the corrosion resistance of liquid metal and prolonging the service life.
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Embodiment 1
[0020] (1) Pretreatment of the metal surface: Grind the metal sample of 15mm×10mm×2mm size with metallographic sandpaper to No. 600, and round all the edges and corners, and then sandblast the metal surface. After cleaning with metal detergent, ultrasonic cleaning and drying in deionized water;
[0021] (2) Melt the optimally designed enamel ingredients at a high temperature of 1400°C, and then water-cooled after full reaction, then ball milled to produce enamel powder. The main component of the enamel is SiO 2 : 58.26%, Al 2 O 3 : 19.2%, CaO: 3.66%, ZrO 2 : 5.29%, B 2 O 3 : 4.66%, Na 2 O: 3.40%, KNO 3 : 5.53%;
[0022] (3) Mix the enamel powder with absolute ethanol, spray it on the metal surface, and sinter the enamel coating on the metal surface at 730℃±10℃ through curing reaction after drying to form an enamel coating of about 40μm.
[0023] The above metal material is martensitic heat-resistant steel, the specific chemical composition is: C: 0.25wt.%, Si: 1.43wt.%, Cr: 10.8wt.%,...
Embodiment 2
[0026] The chemical composition of 9-12% Cr martensitic heat-resistant steel is: C: 0.19wt.%, Si: 1.05wt.%, Cr: 10.05wt.%, Mn: 1.06wt.%, W: 1.19wt.% , Ta: 0.1wt.%, V: 0.2wt.%, Nb: 0.01wt.%, the balance is iron. The other surface treatment processes of the metal are the same as in Example 1.
Embodiment 3
[0028] The chemical composition of 9-12%Cr martensitic heat-resistant steel is: C: 0.15wt.%, Si: 1.23wt.%, Cr: 10.46wt.%, Mn: 0.41wt.%, W: 1.5wt.% , Ta: 0.15wt.%, V: 0.19wt.%, Nb: 0.014wt.%, the balance is iron. The surface treatment process of the metal is the same as in Example 1.
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