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A catalyst continuous impregnation device

A technology of impregnation device and catalyst, which is applied in catalyst activation/preparation, physical/chemical process catalyst, chemical instruments and methods, etc., can solve the problems of low catalyst forming rate, inability to achieve continuous impregnation, etc., and achieve the effect of improving the forming rate

Active Publication Date: 2018-05-18
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is suitable for materials that are loose and easy to transport after impregnation of the catalyst carrier. When the catalyst carrier is highly adhesive after impregnation, it will adhere to the conveying parts, so that the continuous impregnation process cannot be realized; sometimes due to long-term work, the adhesion The material loses moisture and forms hard scale that adheres to the outer wall of the conveying screw conveyor. When the impregnated material is conveyed later, the wet impregnated carrier will be squeezed and damaged, and the molding rate of the catalyst is low.

Method used

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  • A catalyst continuous impregnation device

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Effect test

Embodiment 1

[0065] use as figure 1 The catalyst continuous impregnation device shown has a total length of 2200mm, a height of 1800mm, and a processing capacity of 200kg / h. The impregnation chamber is equipped with screw rods. The motor speed of the mixing part is 55r / min, and the processing capacity is about 450kg / h; The volume of the material tank of the intermediate buffering part is 12L, the valve plate at the bottom of the material tank is opened by pumping, and it is pushed by pneumatic; 5 times / min; the airtight door of the dryer is equipped with a limit switch, and the flash drying method is adopted.

[0066] In the catalyst continuous impregnation device mentioned above, 390kg of alumina carriers were dropped in, and the impregnating solution was Ni(NO 3 ) 2 Aqueous solution, Ni(NO 3 ) 2 The concentration is 49% by weight, a total of Ni (NO 3 ) 2 Aqueous solution 585kg. After passing through the above catalyst continuous impregnation device, drying in a drier at 180°C for ...

Embodiment 2

[0071] use asfigure 1 The catalyst continuous impregnation device shown has a total length of 1600mm, a height of 1400mm, and a processing capacity of 160kg / h. The impregnation chamber is equipped with screw rods. The motor speed of the mixing part is 37r / min, and the processing capacity is about 300kg / h; The volume of the material tank of the intermediate buffer part is 8L, the valve plate at the bottom of the material tank is opened in a rotating manner, and the motor is driven; the volume of the conveying material tank of the conveying part is 6L, and the valve plate at the bottom of the conveying material tank is opened in a rotating manner, driven by a motor, and the conveying frequency is 6 times / min; the airtight door of the dryer is equipped with a limit switch, and the flash drying method is adopted.

[0072] In the catalyst continuous impregnation device mentioned above, 500kg of alumina carrier was dropped in, and the impregnating solution was Ni(NO 3 ) 2 Aqueous s...

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Abstract

The invention relates to a catalyst continuous impregnation device, comprising: an impregnation chamber (4), in which a catalyst carrier and an impregnation liquid are impregnated and mixed; Mixing; intermediate buffer unit (6) for short-term storage of the catalyst from the mixing unit (5); delivery unit (7) for receiving the catalyst in the intermediate buffer unit (6) and delivering it to the subsequent Drying takes place in a dryer (9) in which the catalyst does not move relative to each other in the conveying means (7) and a dryer (9) for drying the catalyst fed through the conveying means (7). The catalyst continuous impregnation device provided by the invention can realize continuous impregnation of the catalyst, realize impregnation and mixing at room temperature during the impregnation process, transport the catalyst carrier without relative movement and wear, reduce fouling phenomenon during the impregnation process, and improve catalyst forming rate.

Description

technical field [0001] The invention relates to the field of catalyst processing, in particular to a catalyst continuous impregnation device. Background technique [0002] In the catalyst preparation process, impregnation is an indispensable process. The purpose of the impregnation process is to impregnate the catalytically active component on the catalyst carrier, so that it is evenly distributed on the surface of the carrier, and then prepare the catalyst product by drying and roasting the carrier with the catalytically active component. [0003] For example, for the treatment of automobile exhaust emissions of HC, CO and NO x The three-way catalytic converter, the preparation process is to make a honeycomb alumina carrier first, and then impregnate the active metal components such as Pd, Pt, Rh on the alumina carrier to prepare a catalyst, which can convert automobile exhaust for H 2 O.CO 2 , N 2 ; Another example is that ammonium polyvanadate is impregnated on the a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J37/02
Inventor 田志鸿侯栓弟张同旺张哲民张久顺何金龙吕庐峰李学锋刘亚林张翊
Owner CHINA PETROLEUM & CHEM CORP