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Carbon nanostructured composite polyurethane foam and its preparation method and use

A technology of carbon nanostructure and composite polyurethane, which is applied in the field of carbon nanostructure composite polyurethane foam, preparation and application, and can solve problems such as harsh process conditions, complicated pretreatment, and materials without far-infrared functions

Active Publication Date: 2016-04-27
营口圣泉高科材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it needs to chemically bond graphene and polyol, the process conditions are harsh, the pretreatment is complicated, and the prepared material has no obvious far-infrared function.

Method used

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  • Carbon nanostructured composite polyurethane foam and its preparation method and use
  • Carbon nanostructured composite polyurethane foam and its preparation method and use
  • Carbon nanostructured composite polyurethane foam and its preparation method and use

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0082] Embodiment 1 provides a kind of preparation method of composite polyurethane foam, and specific condition is:

[0083] In step (2), the second catalyst is ferrous chloride; the mixing mass ratio of porous cellulose and the second catalyst is 1:0.1; the catalytic treatment temperature is 150°C, and the time is 4h; the moisture content in the precursor is 10wt %;

[0084] The process of obtaining the crude product is as follows: heat up to 280°C at a rate of 3°C / min, hold for 2 hours, then heat up to 950°C at a rate of 15°C / min, and hold for 3 hours;

[0085] The pickling temperature is 55°C, and the concentration of hydrochloric acid used in pickling is 4wt%;

[0086] The carbon nanostructure compound obtained in step (2) mainly contains P, Si, Ca, Al, Na, Fe, Mg elements; and the Raman spectrum shows that the peak height ratio of G peak and D peak is 7; there is 2D peak;

[0087] In the step (3), the raw material composition used comprises the following components in...

Embodiment 2

[0090] Embodiment 2 provides a kind of preparation method of complex polyurethane foam, and specific conditions are compared with embodiment 1, and difference only is that in step (3), the addition amount of the carbon nanostructure composite of raw material composition used is 0.1 weight part.

Embodiment 3

[0091] Embodiment 3 provides a kind of preparation method of composite polyurethane foam, and specific conditions are compared with embodiment 1, and difference is only in step (3), the addition amount of the carbon nanostructure composite of raw material composition used is 10 parts by weight.

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Abstract

The invention relates to composite polyurethane foam. The composite polyurethane foam contains a carbon nanostructured compound, the carbon nanostructured compound contains carbon and 0.5-4wt% of first non-carbon non-oxygen substances, the first non-carbon non-oxygen substances comprise one or at least two of a simple substance and compounds of a first non-carbon non-oxygen element, the first non-carbon non-oxygen element is selected from P, Si, Ca, Al and Na, and a peak height ratio of a carbon peak G to peak D in a Raman spectrum of the carbon nanostructured compound is 1-20. Through use of the specific carbon nanostructured compound, a simple mixing process of the specific carbon nanostructured compound and polyether polyol is realized, and then the mixture and polyisocyanate undergo a polymerization reaction so that polyurethane is compounded. The preparation method is free of a carbon nanostructured compound formation process, has simple processes and can realize seamless connection with the existing equipment.

Description

technical field [0001] The invention belongs to the field of polymer materials, and specifically relates to a carbon nanostructure composite polyurethane foam, a preparation method and an application thereof. The carbon nanostructure composite polyurethane foam has a far-infrared function and can be used to make pillows, mattresses, seat cushions, back cushions, Sofas, waist protectors, insoles, bras, car seats, toilet seat cushions or hand warmers emit far infrared rays to play a health care function. Background technique [0002] The full name of polyurethane is polyurethane, which is a general term for macromolecular compounds containing repeated carbamate groups in the main chain. It is formed by addition polymerization of organic diisocyanate or polyisocyanate and dihydroxy or polyhydroxy compounds. [0003] CN104892886A discloses a rigid urethane foam with low smoke emission and its preparation method and application. The polyurethane foam is prepared from a compositi...

Claims

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Application Information

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IPC IPC(8): C08L75/08C08K3/04C08G18/48
Inventor 唐一林张金柱王双成彭文杰刘顶
Owner 营口圣泉高科材料有限公司
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