A kind of light-shielding ceramic and its preparation method
A technology of ceramics and ceramic layers, applied in the field of ceramics, can solve the problems of restricting the production and wider application of shading ceramics, affecting the whiteness and shading degree of ceramic products, and poor environmental test ability, achieving excellent shading effect and low cost , good shading effect
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Embodiment 1
[0035] An embodiment of the light-shielding ceramic of the present invention, the light-shielding ceramic of this embodiment is prepared by the following method:
[0036] (1) Preparation of slurry: the material contained in the low refractive index ceramic layer: 60wt.% SiO 2 , 4wt.% of polyvinyl alcohol, 2wt.% of DOP, 4wt.% of TXA-15 and 30wt.% of ethanol were added to the ball milling tank, and then taken out after ball milling for 36 hours to obtain a low refractive index ceramic slurry; Material contained in the ceramic layer: 60wt.% ZrO 2 , 6wt.% of polyvinyl butyral, 2wt.% of dioctyl ester, 2wt.% of TXA-15 and 30wt.% of ethanol are added to the ball milling tank, ball milled for 8 hours and then taken out to obtain a high refractive index ceramic slurry;
[0037] (2) Powder molding: The low refractive index ceramic slurry and the high refractive index ceramic slurry obtained in step (1) are respectively cast and molded to obtain a low refractive index ceramic green body and a ...
Embodiment 2
[0042] An embodiment of the light-shielding ceramic of the present invention, the light-shielding ceramic of this embodiment is prepared by the following method:
[0043] (1) Preparation of slurry: the material contained in the low refractive index ceramic layer: 80wt.% Al 2 O 3 , 2wt.% of a mixture of polyvinyl butyral and polyvinyl chloride (the mass ratio of polyvinyl butyral and polyvinyl chloride is 1:1), 1wt.% of dioctyl ester, 5wt.% of PMMA and 12wt .% acetone was added to the ball milling tank, and then taken out after 32 hours of ball milling to obtain a low refractive index ceramic slurry; the material contained in the high refractive index ceramic layer: 85wt.% TiO 2 , 2wt.% of polyvinyl chloride, 2wt.% of DOP, 1wt.% of lecithin and 10wt.% of acetone are added to the ball milling tank, and then taken out after ball milling for 48 hours to obtain a high refractive index ceramic slurry;
[0044] (2) Powder molding: the low refractive index ceramic slurry and the high refrac...
Embodiment 3
[0049] An embodiment of the light-shielding ceramic of the present invention, the light-shielding ceramic of this embodiment is prepared by the following method:
[0050] (1) Preparation of slurry: the materials contained in the low refractive index ceramic layer: 85wt.% MgO, 3wt.% acrylic resin, 1wt.% dioctyl resin, 1wt.% lecithin and 10wt.% The butyl carbitol was added to the ball milling tank and taken out after ball milling for 48 hours to obtain a low refractive index ceramic slurry; the material contained in the high refractive index ceramic layer: 60wt.% Si 3 N 4 , 20wt.% of polyvinyl alcohol, 3wt.% of PEG, 5wt.% of PMMA and 12wt.% of toluene are added to the ball mill tank, and then taken out after ball milling for 2 hours to obtain a high refractive index ceramic slurry;
[0051] (2) Powder molding: dry pressing the low refractive index ceramic slurry and high refractive index ceramic slurry obtained in step (1) to obtain a low refractive index ceramic green body and a high...
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