High intensity sweetener composition

A technology of high-intensity sweetener and composition, applied in the field of sweetener composition of sucralose

Inactive Publication Date: 2016-06-29
TALE & LYLE TECH LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Not all particle sizes are readily achievable using t

Method used

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Examples

Experimental program
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example

[0094] In Examples 1-4 below, agglomerated sweetener compositions were prepared by agglomerating maltodextrin (DE=6) and micronized sucralose in a Lodige LFPmini2 agglomerator, wherein the nozzle insert In top spray configuration.

[0095] Example 1 - 30% Sucralose, Whole Sucralose Content Dissolved in Solution

[0096] 143 grams of maltodextrin were placed in a fluidized bed and agglomerated with 600 grams of a solution consisting of 143 grams of maltodextrin, 114 grams of micronized sucralose and 400 grams of water. The procedure operates with the following parameters:

[0097] product temperature

[0098] After all the solution has been sprayed, the pump and heater are turned off and the product is allowed to dry for 1 minute. The finished product is discharged from the chamber and screened through a 1mm screen to remove large particles.

[0099] Example 2 - 30% sucralose, half of the total sucralose content dissolved in liquid, and half of the sucralose ...

example 5

[0111] Example 5 - Properties of agglomerates

[0112] The water content of the agglomerates was determined by Karl Fischer analysis using a Karl Fischer titrator (complex 2 reagent).

[0113] The particle size was measured with a Beckman LS320 laser diffraction analyzer.

[0114] Density was measured with an Erwekadensi-volumeter using 250 ml graduated tubes.

[0115] The samples in the table below (prepared according to Examples 1 to 4 above) were analyzed:

[0116]

[0117]

example 6

[0118] Example 6: Thermal stability of agglomerates

[0119] The resulting agglomerates were exposed to accelerated aging in an oven set at 50°C in airtight packaging to prevent loss of moisture. Samples were periodically removed from the oven and analyzed for pH, color (whiteness and yellowness), sucralose content and 4-chlorogalactose content.

[0120] Sucralose content was determined by HPLC. The samples were previously diluted to 10% concentration (weight / weight) with water adjusted to pH = 6 with diluted sodium hydroxide / hydrochloric acid solution, and then the pH was measured. A rapid drop in pH is an indicator of sucralose degradation. Determine Hunter color with a HunterLab colorimeter. Whiteness and yellowness values ​​can be calculated according to ASTM E313. 4-Chlorogalactose is a by-product of thermal degradation of sucralose. Its content was determined by ion chromatography using separation on a carbohydrate anion exchange column, through a gradient of sodi...

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Abstract

A sweetener composition is described comprising agglomerated particles. The agglomerated particles include one or more core particles which consist of a first carrier substance having a relative sweetness of less than 0.3 and present in an amount of from 45 to 10wt% (based on the weight of the composition). A coating is disposed around the one or more core particles, the coating comprising a second carrier substance having a relative sweetness of less than 0.3 and present in an amount of from 45 to 10wt% (based on the composition weight) and a high intensity sweetener having a relative sweetness of greater than 100 and present in an amount of from 10 to 80wt% (based on the composition weight).

Description

technical field [0001] The present invention relates to sweetener compositions comprising high intensity sweeteners, particularly sucralose. Background technique [0002] Sucralose (sucralose) has the scientific name 4,1',6'-trichloro-4,1',6'-trideoxygalactose (4,1',6'trichloro-4,1', 6'-trideoxy-galacto-surcose) high-intensity sweetener. It has a relative sweetness of about 600. Sucralose and other high intensity sweeteners are often formulated with other materials to provide a more manageable sweetener composition. The other materials are typically carriers which do not contribute significantly to the overall sweetness of the composition, or other sweeteners which do contribute significantly to the overall sweetness of the composition. Other materials such as binders may also be included in the composition. [0003] Such sweetener compositions can be conceptually divided into two types: tabletop products intended for consumer use, and ingredient products intended for us...

Claims

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Application Information

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IPC IPC(8): A23L27/30A23P20/20A23L5/00C07H3/04A23L27/00
CPCA23V2002/00A23P10/20A23L27/33A23L27/37A23V2200/202A23V2200/22A23V2200/254A23V2250/264A23V2250/5114A23L27/70A23L27/30A23P20/00A23P20/15C07H3/04A23L2/60
Inventor 纳瑟莉·维奥莱特·索米耶
Owner TALE & LYLE TECH LTD
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