Preparation method of purified vanadium adsorption material
A technology of adsorption materials and porogens, which is applied in the field of preparation of purified vanadium adsorption materials, can solve the problems of long process route, complex components, and easy introduction of new impurities, etc., to achieve improved adsorption capacity, high adsorption capacity, and not easy to lose Effect
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Embodiment 1
[0020] Step 1. Preparation of water phase
[0021] In parts by weight, add 100 parts of pure water and 0.5 part of polyvinyl alcohol into the reactor, and stir evenly.
[0022] Step 2. Preparation of oil phase
[0023] Mix and stir the oil phase components in the following proportions evenly;
[0024] Component Parts by weight
[0025] Vinylidene chloride 100
[0026] Bis(cyclopentadiene)vanadium iodide 65
[0027] Octadecenedioic acid 33
[0028] 1-allyl-3-butylimidazolium tetrafluoroborate 0.3
[0029] Toluene 30
[0030] Benzoyl Peroxide 2
[0031] Step 3. Polymerization
[0032] Add the prepared oil phase solution in step 2 to the reaction kettle equipped with the prepared water phase in step 1, react at 90°C for 14 hours, discharge the material after the reaction is completed, and extract the toluene after drying to obtain the product. The number is W-1.
Embodiment 2
[0034] Step 1. Preparation of water phase
[0035] In parts by weight, add 100 parts of pure water and 1.5 parts of polyvinyl alcohol into the reactor, and stir evenly.
[0036] Step 2. Preparation of oil phase
[0037] Mix and stir the oil phase components in the following proportions evenly;
[0038] Component Parts by weight
[0039] Vinylidene chloride 100
[0040] Bis(cyclopentadiene)vanadium iodide 50
[0041] Octadecenedioic acid 20
[0042] 1-allyl-3-butylimidazolium tetrafluoroborate 0.1
[0043] white oil 40
[0044] Benzoyl Peroxide 0.5
[0045] Step 3. Polymerization
[0046] Add the prepared oil phase solution to the reaction kettle equipped with the prepared water phase in step 1, react at 80°C for 24 hours, discharge the material after the reaction is completed, and extract the porogen after drying to obtain the product, No. for W-2.
Embodiment 3
[0048] Step 1. Preparation of water phase
[0049] In parts by weight, add 100 parts of pure water and 2 parts of polyvinyl alcohol into the reactor, and stir evenly.
[0050] Step 2. Preparation of oil phase
[0051] Mix and stir the oil phase components in the following proportions evenly;
[0052] Component Parts by weight
[0053] Vinylidene chloride 100
[0054] Bis(cyclopentadiene)vanadium iodide 90
[0055] Octadecenedioic acid 50
[0056] 1-allyl-3-butylimidazolium tetrafluoroborate 0.5
[0057] Mineral spirits 20
[0058] Benzoyl Peroxide 3
[0059] Step 3. Polymerization
[0060] Add the prepared oil phase solution to the reaction kettle equipped with the prepared water phase in step 1, react at 110°C for 10 hours, discharge the material after the reaction is completed, and extract the porogen after drying to obtain the product, No. for W-3.
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