Processing method of modified Artemisia sphaerocephala Krasch gum emulsifier
A processing method and technology of Artemisia gum, which is applied in the field of preparation of Artemisia gum emulsifiers, can solve the problems of low yield, unstable emulsification, and high extraction cost of Artemisia gum, so as to improve the emulsification effect and shorten the drying time , good emulsification stability
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[0021] Example 1
[0022] In this example, 1kg of Artemisia sphaerocephala seeds was used as raw material, and the Artemisia sphaerocarpa gum emulsifier was prepared through three steps of hot lye extraction, neutralization and desalination, and spray drying. The specific process is:
[0023] (1) Hot water extraction
[0024] Soak 1 kg of Artemisia sphaerocephala seeds in 20 kg of NaOH solution with a concentration of 0.5 mol / L, and extract for 2 h at 70° C. with constant stirring, separate the extract, and let stand for 1 h to separate into layers.
[0025] (2) Neutralization and desalination
[0026] Take the supernatant and adjust it to neutral with a concentration of 1mol / L HCl solution, and carry out continuous ultrafiltration and concentration treatment on the neutralized liquid. The molecular weight cut-off of the filter membrane is 20000~30000Da, the control pressure is 0.5MPa, and the temperature is At 80°C, remove excess salt to obtain a high-concentration solution of Artemis...
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[0029] Example 2
[0030] In this example, 1kg of Artemisia sphaerocephala seeds was used as raw material, and the Artemisia sphaerocarpa gum emulsifier was prepared through three steps of hot lye extraction, neutralization and desalination, and spray drying. The specific process is:
[0031] (1) Hot water extraction
[0032] 1kg of Artemisia sphaerocephala seeds were immersed in 18kg of 0.5mol / L NaOH solution, extracted at 60°C for 4h, and continuously stirred to separate the extract, stand for 1.5h, and layer.
[0033] (2) Neutralization and desalination
[0034] Take the supernatant and adjust it to neutral with a concentration of 1mol / L HCl solution, and carry out continuous ultrafiltration and concentration treatment on the neutralization solution. The molecular weight cut-off of the filter membrane is 10000~30000Da, the control pressure is 0.3MPa, and the temperature is At 70°C, remove the salt in the concentrated solution to obtain a high-concentration solution of Artemisia Gum....
Example Embodiment
[0037] Example 3
[0038] In this example, 1kg of Artemisia sphaerocephala seeds was used as raw material, and the Artemisia sphaerocarpa gum emulsifier was prepared through three steps of hot lye extraction, neutralization and desalination, and spray drying. The specific process is:
[0039] (1) Hot water extraction
[0040] 1 kg of Artemisia sphaerocephala seeds were immersed in 25 kg of NaOH solution with a concentration of 0.5 mol / L, and extracted at 80° C. for 2 hours with constant stirring. The extract was separated and stood for 1.5 hours to separate layers.
[0041] (2) Neutralization and desalination
[0042] Take the supernatant liquid and adjust it to neutral with a concentration of 1mol / L HCl solution, and carry out continuous ultrafiltration and concentration treatment on the neutralized liquid. The molecular weight cut-off of the filter membrane is 10000~25000Da, the control pressure is 0.8MPa, and the temperature is Remove excess salt at 90°C to obtain a high-concentrati...
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