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137 results about "Sodium ascorbate" patented technology

Sodium ascorbate is one of a number of mineral salts of ascorbic acid (vitamin C). The molecular formula of this chemical compound is C₆H₇NaO₆. As the sodium salt of ascorbic acid, it is known as a mineral ascorbate. It has not been demonstrated to be more bioavailable than any other form of vitamin C supplement.

Synthetic nicotine composition and preparation method thereof

The invention relates to the technical field of pharmaceutical preparations, and particularly discloses a synthetic nicotine composition and a preparation method thereof. The nicotine buccal film agent disclosed by the invention is prepared from the following components in parts by weight: 2 to 4 parts of nicotine clathrate compound powder, 0.2 to 0.6 part of phosphatidic acid, 0.1 to 0.3 part of tannic acid, 0.1 to 0.2 part of sodium ascorbate, 0.04 to 0.06 part of tocopherol, 0.01 to 0.02 part of ethylene diamine tetraacetic acid, 2 to 4 parts of povidone and 40 to 80 parts of absolute ethyl alcohol. The synthesized nicotine composition prepared by the invention can effectively relieve the phenomenon that the faster the nicotine is released, the stronger the bitter taste is. Meanwhile, in a high-temperature and high-humidity environment, the stability of nicotine can be effectively maintained, and the oxidation half-life period of nicotine is prolonged.
Owner:MAOMING TIANXI BIOTECHNOLOGY CO LTD

Purification method of eugenol

The invention relates to the technical field of separation and purification, in particular to a purification method of eugenol, which comprises the following steps: (a) dissolving crude eugenol in an ethanol aqueous solution to prepare a solution with eugenol mass concentration of 20-30%; (b) adding a composite protective agent into the solution, uniformly stirring and standing to obtain a mixed solution, the composite protective agent comprising modified chitosan, sodium ascorbate and nano-silica; (c) carrying out reduced pressure evaporation on the mixed solution, and recovering the solvent to obtain a concentrated solution; (d) adding the concentrated solution into a glycine aqueous solution with the mass concentration of 1-2%, uniformly stirring and standing; and (e) carrying out segmented temperature control rectification on the concentrated solution treated in the step (d), and collecting a target fraction to obtain the high-purity eugenol. By introducing a novel protective agent system and a staged temperature control rectification technology, the occurrence rate of thermal decomposition and oxidation reaction is remarkably reduced, and the product purity and the production efficiency are improved.
Owner:JIANGXI HAIRUI NATURAL PLANT CO LTD

Application of corn germ concentrated powder in improvement of osteoarthritis

The invention belongs to the technical field of food and medicine, and relates to application of corn germ concentrated powder in improvement of osteoarthritis. The invention particularly relates to application of corn germ concentrated powder, namely corn antioxidant multienzyme, in preparation of medicines or health-care foods for treating rheumatoid arthritis and osteoporosis. In the corn germ concentrated powder, superoxide dismutase / (U / g) is greater than or equal to 8500, glutathione peroxidase / (U / g) is greater than or equal to 5000, and catalase / (U / g) is greater than or equal to 750. The corn germ concentrated powder can also be prepared by the following method: cleaning corn, germinating, adding water into the germinated corn, grinding and pulping, adding a settling agent into the corn steep liquor, standing, taking supernate, adding part of sodium ascorbate, performing temperature-controlled concentration, adding the rest sodium ascorbate and a stabilizer into the concentrated solution, and uniformly mixing to obtain the corn germ concentrated powder. And drying at controlled temperature, crushing, and mixing with a proper amount of silicon dioxide. The prepared corn germ concentrated powder has the effect of resisting rheumatoid arthritis.
Owner:LIAONING PROSPECTIVE BIOTECH

Radiopharmaceutical compositions for low toxicity actinium in targeted radionuclide therapy

The present disclosure provides a high-energy, low toxicity radiopharmaceutical composition comprising actinium that performs as an anti-tumor agent for targeted radionuclide therapy and has improved shelf-life stability. Specifically, the radiopharmaceutical composition may include 225Ac-PSMA I&T, sodium ascorbate, and optionally hydrochloric acid. The radiopharmaceutical composition may be suitable for administration to a patient in need thereof, such as for the purpose of treating prostate cancer.
Owner:CURIUM US LLC

Food-grade metal surface blackening liquid, blackening process and application

The invention discloses food-grade metal surface blackening liquid as well as a blackening process and application. The blackening liquid comprises a basic blackening component and a modified graphene solution, wherein the basic blackening liquid comprises 15-25 g / L of sodium pyrophosphate, 8-12 g / L of sodium molybdate, 20-30 g / L of sodium gluconate, 2-5 g / L of sodium erythorbate, a citric acid / sodium citrate buffer solution, 10-15 ml / L of polyethylene glycol and 0.5-1 ml / L of polysorbate 80; the modified graphene is PEI modified graphene oxide. According to the method, stubborn dirt is cleaned and peeled off through ultrasonic waves, and grease is degraded through photocatalysis of nano TiO2, so that the surface hydrophilicity is improved, and the adsorption uniformity of blackening liquid is enhanced; according to the method, Si-O-Si network crosslinking is optimized through staged heating (80 DEG C to 120 DEG C to 140 DEG C), the hardness and the adhesive force are improved, thermal stress concentration in a traditional process is avoided, meanwhile, raw material decomposition can be avoided at the temperature, and the safety of blackening liquid is further guaranteed.
Owner:GUANGDONG CANBO ELECTRICAL

Comprehensive recovery method for antimony-containing gold concentrate

The invention belongs to the technical field of metallurgy, and relates to a comprehensive recovery method for antimony-containing gold concentrate, which comprises the following steps: S1, mixing antimony-containing gold concentrate and an antioxidant, carrying out size mixing, then adding sodium sulfide and sodium hydroxide to obtain a size, and reacting to obtain a leaching solution and leaching residues; s2, the leachate obtained in the step S1 is subjected to electrodeposition, and crude antimony and barren liquor are obtained; wherein in the step S1, the antioxidant is a mixture of sodium ascorbate and ethylenediamine tetraacetic acid disodium salt. According to the method, the antimony-containing gold concentrate is subjected to antimony leaching through Na2S under the alkaline condition, in order to avoid gold loss caused by the fact that S < 2-> is oxidized into S < x > < 2-> and then the S < x > < 2-> and Au generate AuSx dissolved in an alkaline solution in the leaching process, an antioxidant is added in the leaching process, leaching of gold in the antimony-containing gold concentrate can be remarkably reduced, and the recovery rate of gold is increased.
Owner:SHANDONG HUMON SMELTING

Preparation method of high-temperature-resistant and photolysis-resistant composite pigment and application of composite pigment in meat products

The invention relates to the technical field of preparation of composite pigments, in particular to a preparation method of a high-temperature-resistant photolysis-resistant composite pigment and application of the high-temperature-resistant photolysis-resistant composite pigment in meat products. According to the technical scheme, the method comprises the following steps: preparing the following raw materials in parts by weight: pigment base materials: 5-18 parts of monascus red pigment, 4-12 parts of high-color-value capsanthin and 3-8 parts of beta-cyclodextrin embedded curcumin; the component A comprises the following components in parts by weight: 1-5 parts of ascorbyl palmitate, 2-8 parts of polyglycerol fatty acid ester, 0.5-3 parts of L-sodium ascorbate and 0.1-1.5 parts of nano titanium dioxide; and 1 to 4 parts of N-acetyl-L-cysteine. The ultra-high stability of the natural pigment under the conditions of high-temperature processing and strong light irradiation is realized, the processing tolerance and the final color development effect are balanced, the problem of uneven dyeing caused by early release of the traditional pigment is solved, the product quality and the application convenience are improved, and the unification of safety and efficacy is realized.
Owner:GOLDEN MILL FOOD CO LTD

Salad dressing capable of improving stability of natural pigment and preparation method of salad dressing

The invention belongs to the technical field of seasoning processing, and particularly discloses salad dressing capable of improving the stability of natural pigments and a preparation method of the salad dressing. The salad dressing capable of improving the stability of the natural pigment comprises the following raw materials: high fructose corn syrup, yolk liquid, white granulated sugar, potassium sorbate, lemon concentrated juice, table vinegar, water, glycerol, the natural pigment, titanium dioxide, sucrose fatty acid ester, edible salt, xanthan gum, soybean oil, acetylated distarch adipate, sodium ascorbate, mustard powder and a rosemary extract. The HLB (Hydrophile Lipophile Balance) value of the sucrose fatty acid ester is The synergistic effect of all the components is remarkable, multiple defense lines of oxidation resistance, system stability, corrosion prevention and the like are constructed, and the probability of natural pigment fading in the salad dressing storage process is reduced.
Owner:FUJIAN HECHUAN TECH CO LTD

Fat-soluble component nano-emulsion and preparation method thereof

The invention relates to the technical field of preparation of health-care products, in particular to a fat-soluble component nano-emulsion and a preparation method thereof. The preparation method comprises the following steps: stirring and dissolving the antioxidant and the caprylic / capric triglyceride, adding the vitamin D3 and the retinyl palmitate, and stirring and dissolving to obtain an oil phase; stirring the starch sodium octenylsuccinate in purified water until the starch sodium octenylsuccinate is dissolved, adding glycerol, and uniformly stirring and mixing to obtain a water phase; adding a small amount of water phase into the oil phase, and stirring at high speed to obtain primary emulsion; adding the primary emulsion into the residual water phase, stirring at a high speed, shearing and homogenizing to obtain a nano embedding emulsion; adding citric acid, cane sugar and sodium ascorbate into purified water, adding the nano embedding emulsion, and uniformly stirring to obtain a concentrated solution; and diluting the concentrated solution and adjusting the pH value to obtain the fat-soluble component nano-emulsion. The fat-soluble component nano-emulsion provided by the invention has good safety; the product can be easily absorbed and utilized by a human body, and is convenient for people to quickly supplement vitamin A and vitamin D3 required by the body.
Owner:HEILONGJIANG RENHETANG PHARM CO LTD

A rice nano-flavor enhancer and its application in rice cultivation

ActiveCN119214166BBiocidePlant growth regulatorsBiotechnologyAromatic rice
This invention belongs to the field of crop cultivation technology, specifically relating to a rice nano-flavor enhancer and its application in rice cultivation. The rice nano-flavor enhancer of this invention is prepared from raw materials such as sodium octenyl succinate starch, sodium ascorbate, and sodium selenite. The prepared octenyl succinate starch-nano-selenium has advantages such as small nanoparticle size and system stability. This flavor enhancer can not only significantly improve the overall aroma of fragrant rice, but also enhance the aroma of non-fragrant rice. Specifically, it can significantly increase the content of volatile aroma compounds such as 2-acetyl-1-pyrroline (2-AP) in fragrant rice grains, and significantly increase the content of volatile aroma compounds such as vanillin, benzaldehyde, and geranylacetone in non-fragrant rice grains. Unlike traditional rice flavor enhancers, the rice nano-flavor enhancer of this invention has better applicability and a wider range of applications, helping to meet the growing market demand for high-quality rice.
Owner:WUHAN POLYTECHNIC UNIVERSITY

Method for detecting extracellular vesicle fusion by adopting fluorescence resonance energy transfer

The invention provides a method for detecting fusion of extracellular vesicles by adopting fluorescence resonance energy transfer, and belongs to the technical field of extracellular vesicles. A dynamic fluorescence monitoring system is established, low-power laser excitation is adopted, dual-wavelength fluorescence signals are monitored at the same time, fluorescence signal data are collected, graded gain regulation and control processing is carried out through five threshold values, and a fluorescence signal super-sparse matrix is constructed; establishing a fluorescence signal processing matrix model, converting the super-sparse matrix into a dense matrix, constructing a gain matrix for signal correction, calculating a fluorescence resonance energy transfer efficiency parameter, obtaining a standardized efficiency value through matrix operation, outputting an extracellular vesicle fusion kinetic analysis result, and establishing a quantitative evaluation system. The technical problems of poor signal stability and low detection precision in the process of fluorescence resonance energy transfer detection of extracellular vesicle fusion are solved.
Owner:QINGDAO RAISECARE BIOTECHNOLOGY CO LTD

Thin-layer chromatography separation method and detection method for amino polyether and matrix in fluorine-18 labeled radiopharmaceutical

The invention relates to the technical field of thin-layer chromatography detection, and discloses a thin-layer chromatography separation method for amino polyether and a matrix in a fluorine-18 labeled radiopharmaceutical, and the adopted developing solvent is acetonitrile and ammonia water, and the volume ratio of the acetonitrile to the ammonia water is 90: 10-85: 15. According to the method, amino polyether and matrix components are separated by adopting a developing solvent with a specific volume ratio, and particularly, sodium ascorbate in the amino polyether and the matrix is separated.
Owner:GUOTONG (CHENGDU) NEW DRUG TECH CO LTD

Radiopharmaceutical compositions for low toxicity actinium in targeted radionuclide therapy

The present disclosure provides a high-energy, low toxicity radiopharmaceutical composition comprising actinium that performs as an anti-tumor agent for targeted radionuclide therapy and has improved shelf-life stability. Specifically, the radiopharmaceutical composition may include 225Ac-PSMA I&T, sodium ascorbate, and optionally hydrochloric acid. The radiopharmaceutical composition may be suitable for administration to a patient in need thereof, such as for the purpose of treating prostate cancer.
Owner:CURIUM US LLC

Vacuum color protection method for preserved apples

The invention discloses a vacuum color protection method of preserved apples, which comprises the following steps: peeling apples, removing kernels, and cutting the apples into apple slices; soaking the apple slices in a composite color-protecting solution, performing vacuum-pumping treatment, and continuing soaking to obtain the preserved apples subjected to color-protecting treatment; the composite color protection liquid is composed of citric acid, sodium erythorbate, sodium chloride, calcium chloride and water, the concentration of the citric acid is 3-6%, the concentration of the sodium erythorbate is 0.3-0.5%, and the concentration of the sodium chloride is 0.3-0.5%. The color fixative disclosed by the invention is combined with a vacuum mode, so that a greater benefit effect is exerted, and the color protection effect is improved under the condition that the water activity is not influenced. The method is simple in process and convenient to operate, toxic and harmful chemicals are not added, and the method has wide application and popularization prospects.
Owner:JIANGNAN UNIV +1

Automatic preparation and dosing system for sodium erythorbate deoxidant

The utility model belongs to the technical field of dosing devices, and particularly relates to an automatic preparing and dosing system for a sodium erythorbate deoxidant. Comprising a sodium erythorbate storage tank, a preparation tank, a dosing pump, a deaerator and a water feeding pump which are connected in sequence, a top outlet of the sodium erythorbate storage tank is connected with a pressure relief pipeline, the pressure relief pipeline is provided with a back flushing type filter, a bottom outlet of the sodium erythorbate storage tank is connected with an electric rotary feeding valve and a weighing sensor, and the weighing sensor is connected with the sodium erythorbate storage tank. The preparation tank is connected with a desalted water pipeline; an online dissolved oxygen analyzer is arranged at an outlet of the deaerator; an outlet of the nitrogen pipeline is respectively connected with inlet pipelines of the back flushing type filter, the sodium erythorbate storage tank and the preparation tank through pipelines; a control system is further included. And through precise control, the deoxygenation requirement is met. On-line monitoring and automatic adjustment are combined, the dissolved oxygen index is stabilized within the preset range, fluctuation caused by manual adjustment is effectively avoided, the running stability of a downstream boiler is remarkably improved, and meanwhile the working efficiency is improved.
Owner:TIANCHEN QIXIANG NEW MATERIAL CO LTD

Rifapentine isoniazide tablet and preparation method thereof

The invention discloses a rifapentine isoniazide tablet and a preparation method thereof, the rifapentine isoniazide tablet is a core-coated tablet, and comprises an inner-layer tablet core containing rifapentine and an outer-layer tablet layer containing isoniazide; the inner-layer tablet core comprises rifapentine, edetate disodium, sodium ascorbate and lauryl sodium sulfate, the rifapentine accounts for 53-63% of the total mass of the inner-layer tablet core, and the rifapentine tablet further comprises a filler, a stabilizer, a disintegrating agent, an adhesive, a surfactant, a lubricant and a coating layer; the coating layer coats the inner-layer tablet core; the outer sheet layer comprises isoniazide, a filling agent, a disintegrating agent, an adhesive, a lubricant and an adhesive; and the mass of the isoniazide accounts for 75-95% of the total mass of the outer sheet layer. According to the rifapentine isoniazide tablet disclosed by the invention, the compliance of a patient is enhanced. And meanwhile, the potential safety hazard problem of impurity increase caused by incompatibility of rifapentine and isoniazide is solved.
Owner:ZHUOHE PHARM GRP CO LTD

Fat powder free of starch sodium octenylsuccinate, protein and lactose as well as preparation method and application of fat powder

The invention provides starch sodium octenylsuccinate-free, protein-free and lactose-free fat powder as well as a preparation method and application thereof, and belongs to the technical field of foods. The fat powder provided by the invention comprises 25%-60% of glucose syrup (in terms of solid matter), 1%-20% of maltodextrin, 20%-50% of edible plant blend oil, 0.01%-3% of mono-and diglycerol fatty acid ester, 0.01%-3% of citric acid fatty glyceride, 0.1%-1% of sodium ascorbate, 0.005%-0.02% of ascorbyl palmitate and 0.01%-1% of potassium hydroxide. The fat powder provided by the invention is free of starch sodium octenylsuccinate, protein and lactose, good in solubility, good in dispersity and high in sinking speed. After being dissolved, the emulsion is milky white, has no (or few) small oil droplet floating, no precipitate and no floating object, and after standing, the solution is not layered.
Owner:HEBEI DONGKANG DAIRY CO LTD

Substrate additive for sequencing and application thereof

The invention relates to the technical field of gene sequencing, in particular to a substrate additive for sequencing and application of the substrate additive. Wherein the stabilizer comprises potassium citrate, sodium salicylate, chitosan, sodium ascorbate, vitamin E, epigallocatechin gallate, glutathione, cysteine or a derivative thereof. The substrate additive provided by the invention can prevent a substrate from being oxidized to a certain extent and releasing free radicals, and can remove the free radicals generated in the reaction process, so that the substrate is more stable, and meanwhile, the generated free radicals are prevented from damaging to-be-detected DNA molecules, so that the sequencing quality is effectively improved.
Owner:MGI TECH CO LTD

A preparation method of sodium D-isoascorbate

The invention relates to a method for preparing sodium D-isoascorbate. The method comprises the following steps: loading polyoxometalate and polydopamine on silica microspheres to obtain silica microspheres loaded with polyoxometalate; dissolving a 2-keto-D-gluconic acid concentrate with methanol, then adding H2O2 and the silica microspheres loaded with polyoxometalate and heating to carry out an esterification reaction; after completion of the reaction, filtering and separating the silica microspheres loaded with polyoxometalate under a heat preservation condition, cooling, crystallizing, and filtering to obtain 2-keto-D-gluconate; adding 2-keto-D-gluconate to methanol to obtain a methanol solution of 2-keto-D-gluconate, then gradually adding an alcohol solution of a sodium ion donor to carry out a conversion reaction, and after completion of the reaction, filtering, cooling, and centrifuging to obtain the product. The method has high production safety and high product yield.
Owner:NEW TUOYANG BIO-ENG CO LTD

Application of sodium erythorbate in octopus storage and octopus storage method

According to the application of the sodium isoascorbate in octopus storage and the octopus storage method, the sodium isoascorbate is used for inhibiting the reduction of the content of sulfydryl in octopus bodies, delaying the content of carbonyl and the increase of the activity of Ca < 2 + >-ATPase, and effectively reducing the adverse change in the freezing and thawing process, so that the denaturation of protein is reduced, and the storage effect of the octopus is improved. The quality of the frozen and thawed octopuses can be kept to the maximum extent, and the octopus freeze-thawed food has high freezing resistance and is safer and more effective.
Owner:FISHERIES RESEARCH INSTITURE OF FUJIAN

Novel air regulating agent and preparation process thereof

PendingCN121942757ARelease rate dynamic synchronizationdynamic sync release rateDispersed particle separationEdible seed preservationSodium ascorbateEthylic acid
The invention relates to the technical field of air conditioning agents, and discloses a novel air conditioning agent and a preparation process thereof, the novel air conditioning agent is prepared from the following raw materials by mass: 10.0-20.0% of light calcium carbonate; 25.0% to 32.5% of D-sodium erythorbate; 5.0%-15.0% of an odor absorbing agent; 0.5%-2.0% of ferrous acetate; 1.0%-3.0% of sodium carbonate; 0.5%-1.5% of citric acid; 15.0% to 20.0% of sodium-based montmorillonite; 5.0% to 10.0% of silicon dioxide; 1.5% to 4.5% of an anti-flocculation synergist; and the balance of water. The device realizes stable air pressure in a reaction period and low-temperature quick effect, effectively absorbs and removes peculiar smell, solves the hardening problem in water-containing material production, and is suitable for industrial continuous production.
Owner:BEIJING YINGFENG LITAI TECH TRADE +1

Vitamin D3 inclusion compound, preparation thereof, and preparation method thereof

The present invention discloses a vitamin D 3 inclusion compound and a preparation method thereof. The present invention also discloses calcium carbonate D 3 tablets containing the vitamin D 3 inclusion compound and a preparation method thereof. The vitamin D3 inclusion compound of the present invention is calculated by mass percentage and includes: 0.05~0.75% vitamin D3; 80.00~92.25% hydroxypropyl-β-cyclodextrin; 1.00~10.00% antioxidant; 0.00~5.00% anti-adherent; wherein the antioxidant is butylated hydroxytoluene (BHT), vitamin E and sodium ascorbate. The present invention also provides a preparation method of the vitamin D 3 inclusion compound. The vitamin D 3 inclusion compound prepared by the present invention has a high inclusion rate, a high yield, and can be stored stably for a long time. The preparation prepared with the inclusion compound (such as calcium carbonate D 3 tablets) meets pharmaceutical requirements, has good long-term stability, high uniformity, is simple to prepare, and has low cost.
Owner:REGENEX PHARMA LTD

3n-PTD ligand, and preparation method and application thereof

The application belongs to the technical field of extraction separation, and particularly relates to a 3N-PTD ligand and a preparation method and application thereof. The preparation method provided by the application comprises the following steps: mixing 3-chloropropylamine hydrochloride, sodium azide and deionized water, and performing a reflux reaction to obtain 3-azidopropylamine; dissolving 2,6-diethynylpyridine, 3-azidopropylamine, sodium ascorbate and CuSO4.5H2O, and performing a click reaction to obtain the 3N-PTD ligand. The yield of the 3N-PTD ligand obtained by the preparation method is high.
Owner:LANZHOU UNIV

Braised pepper sauce and preparation method thereof

The invention relates to the technical field of food processing, and discloses a roasted pepper sauce and a preparation method thereof. The roasted chili sauce comprises the following raw material components: a chili main material, an auxiliary material, a seasoning, a natural pigment and an antioxidant, wherein the chili main materials comprise red chilies, green chilies and yellow chilies; the auxiliary materials comprise a scorch aroma excitation auxiliary material and a flavor balance auxiliary material; the seasonings comprise ginger, garlic, salt and zanthoxylum oil; the antioxidant is selected from at least one of rosemary extract, tea polyphenol and sodium ascorbate. The preparation method of the roasted chili sauce is simple and controllable, the preparation process is standardized, the chili main material is cut into sections, then the chili sections are subjected to far infrared heating treatment, and then other raw materials are mixed, so that harmful substances and residues of tar, carbon black and the like caused by local high temperature are avoided, and the prepared roasted chili sauce is rich in scorch aroma flavor, rich in taste and rich in flavor. The color, the taste and the quality stability are good, and industrial production and market popularization are facilitated.
Owner:DONGGUAN HUAJING BIOTECHNOLOGY CO LTD

PH test composition, pH test tablet containing pH test composition and application of pH test composition and pH test tablet

The invention provides a pH test composition, a pH test tablet containing the pH test composition and application. The pH test composition comprises a pH indicator, a dechlorinating agent and an additive, wherein the dechlorinating agent comprises any one or a combination of at least two of sodium thiosulfate, sodium sulfite or sodium ascorbate. The dechlorinating agent is added into the pH testing composition, so that the original pH detection is not influenced, the detection sensitivity and the detection precision of the pH in the chlorine-containing water phase to be detected can be improved, and the pH testing composition can be applied to pH detection of swimming pool water and tap water and has a wide application prospect.
Owner:NANJING YIMU INTELLIGENT TECHNOLOGY CO LTD

Process for preparing instant BCAA powder

The invention relates to the technical field of medicinal preparations, in particular to a process for preparing instant BCAA powder, which comprises the following steps: (1) pretreatment: crushing a BCAA mixture until the particle size is 12-18 [mu] m, the ratio of leucine to isoleucine to valine in the BCAA mixture is 2.2: 1: 0.8; (2) mixing: putting 55-65% by mass of a composite instant auxiliary material, 2-4% by mass of a compound emulsifier, 1-3% by mass of sodium ascorbate, 1-2% by mass of a flavoring agent and 0.5-1% by mass of silicon dioxide into a three-dimensional mixer, mixing for 10min at 150r / min, then adding 20-30% by mass of the pretreated BCAA powder, and continuously mixing for 15min to obtain the premix. By optimizing the whole process of pretreatment, mixing, granulation, drying and screening, multi-dimensional improvement of instant solubility, anti-caking property, activity retention, taste, production efficiency and use convenience is realized. Compared with the prior art, the process has the advantages that the BCAA powder which is quick to dissolve, less in caking, high in activity and good in taste can be produced, the production efficiency is high, the cost is low, and the use scene is wide.
Owner:PUHUI RUIXIN (CHANGZHOU) NUTRITION TECH CO LTD

Method for non-targeting screening of hydroxyl esterification-derived glucocorticoids in cosmetics by using low-resolution mass spectrometry

The invention discloses a method for non-targeting screening of hydroxyl esterification-derived glucocorticoid in cosmetics by using a low-resolution mass spectrum, which specifically comprises the following steps: adding sodium hydroxide with the concentration of 10 mg / mL into an acetonitrile solvent system under an alkaline condition, and adding a quantitative stabilizer consisting of EDTA (Ethylene Diamine Tetraacetic Acid) and sodium ascorbate into a reaction system, the method comprises the following steps: controlling the reaction time at room temperature to be 1 hour, adding an acetonitrile aqueous solution containing acetic acid to adjust the reaction system to be in an acidic environment and metering the volume, performing hydrolysis deesterification on glucocorticoids derived from different esterification of hydroxyl groups at 21 site and (or) 17 site of a D ring, returning to the state before esterification and derivation, and enabling the product to be stable; furthermore, only one kind of hydroxyl esterification-free glucocorticoid is adopted as a standard substance, and the hydroxyl esterification-derived glucocorticoid in cosmetics can be screened in a non-targeted manner through high performance liquid chromatography-tandem triple quadrupole mass spectrometry.
Owner:大连市检验检测认证技术服务中心

A method for purifying sodium D-erythorbate

The application provides a purification method of sodium D-erythorbate, which comprises the following steps: (1) adding dimethyl carbonate into a reaction kettle, adding a catalyst, and then adding 2-keto-D-gluconic acid, so as to obtain an esterification liquid through reaction; (2) adding an inorganic base into the esterification liquid obtained in the step (1) and reacting for 1-2 hours, so as to obtain a reaction liquid; (3) filtering the reaction liquid obtained in the step (2), so as to obtain a filtrate and a filter cake, and the filter cake is the catalyst; (4) heating and reducing-pressure distilling the filtrate obtained in the step (3), so as to obtain methanol, dimethyl carbonate and a remaining component which is a crude product of sodium D-erythorbate, respectively; and (5) purifying the crude product of sodium D-erythorbate obtained in the step (4), so as to obtain a pure product of sodium D-erythorbate with a purity of more than 99.8%. The method does not use concentrated sulfuric acid, is simple in process and convenient in operation, has high environmental friendliness of solvents used in the purification process, is high in product purity and can well solve the problems of the prior art.
Owner:NEW TUOYANG BIO-ENG CO LTD

Whitening and brightening composition and cosmetic thereof

The invention discloses a whitening and brightening composition and a cosmetic thereof. The whitening and brightening composition is prepared from ascorbyl tetraisopalmitate, tranexamic acid, Brigtenyl, LightSKN CN, a resveratrol fermentation product, fermented lotus essence and super vitamin A, brigtenyl is a mixture composed of a first solvent, glycerin and diglucosyl gallic acid; lightSKN CN is a mixture composed of a second solvent, 1, 3-propylene glycol, xanthophyll, lecithin, sodium ascorbate and vitamin E; the resveratrol fermentation product is a mixture composed of a third solvent, a pichia pastoris fermentation lysate filtrate and resveratrol; the fermented lotus seed essence is a mixture composed of a fourth solvent, butanediol and a lotus seed extract; the super vitamin A is a mixture of isosorbide dimethyl ether and hydroxyl pinacolone retinoate. The whitening and brightening composition not only can inhibit melanin generation, reduce melanin transfer and accelerate melanin metabolism, but also can remove excessive free radicals in skin, so that the effects of long-acting skin whitening and skin brightening are achieved.
Owner:GUANGDONG BASONA BIOTECHNOLOGY CO LTD

Preparation method of silicon quantum dot-Fe < 3 + > fluorescent probe and application of silicon quantum dot-Fe < 3 + > fluorescent probe in detection of glyphosate pesticide residues

The invention discloses a preparation method of a silicon quantum dot-Fe < 3 + > fluorescent probe and application of the silicon quantum dot-Fe < 3 + > fluorescent probe in detection of glyphosate pesticide residues, belongs to the field of analytical chemistry, and solves the problems that an existing detection method is long in detection time consumption, complex in sample pretreatment and difficult in high-throughput analysis. The preparation method comprises the following steps: introducing a newly prepared sodium ascorbate solution and a 3-aminopropyltrimethoxysilane solution into ultrapure water for reaction; dialyzing the solution in distilled water to remove unreacted solvent, and storing the obtained solution in a dark place at room temperature; carrying out rotary evaporation on the solution until the solution is viscous, pumping by a vacuum pump until the solution is dry, and dissolving by distilled water to obtain a silicon quantum dot solution; and incubating the silicon quantum dot solution and Fe < 3 + > at room temperature to form the silicon quantum dot-Fe < 3 + > fluorescent probe. The preparation method is simple, and reaction products are easy to separate and purify; the method is simple and convenient in glyphosate detection operation, good in selectivity, rapid in response and high in sensitivity, and can be used for rapid and quantitative detection of glyphosate pesticide residues in vegetables.
Owner:LANZHOU INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES