High-inoxidizability lutein microcapsules and preparation method thereof

A technology of anti-oxidation and lutein, which is applied in the direction of microcapsule preparation, microsphere preparation, microcapsules, etc., can solve the problems affecting the storage and transportation of lutein, the complicated preparation method of microcapsules, and the loss of biological activity. Effect of improving oxidation stability and prolonging product shelf life

Active Publication Date: 2016-06-15
江苏九如食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, due to the conjugated polyene structure of lutein, its chemical stability is poor, and it is easily degraded by oxygen, light, temperature, etc., making it lose its biological activity, which affects the storage and transportation of lutein; , Lutein is insoluble in water, slightly soluble in oil and fat
The above factors greatly limit the scope of application of lutein
[0004] U.S. Patent No. 6,863,914 discloses a preparation method of a stable water dispersion of lutein substances and a stable water-dispersible dry powder. The method dissolves lutein in a mixed solution of an organic solvent and water, so the method has an organic solvent Residual problems, not suitable for use in food and pharmaceutical industries
Chinese patent 200610049837 discloses a lutein microcapsule and its preparation method. The preparation method of the microcapsule is complicated and the raw material cost is high

Method used

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  • High-inoxidizability lutein microcapsules and preparation method thereof
  • High-inoxidizability lutein microcapsules and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A lutein microcapsule with strong antioxidative properties, which is prepared from the following components in mass percentage:

[0037] Lutein Crystals 1%

[0038] Sunflower Oil 5%

[0039] Starch Sodium Octenylsuccinate 60%

[0040] Lactose 33.4%

[0041] L-Ascorbyl Palmitate 0.6%.

[0042] The specific preparation method is as follows:

[0043] a. Put lutein crystals into sunflower oil, mix and stir until uniformly dispersed, and prepare an oil phase solution under the conditions of a melting temperature of 150°C and a melting time of 2 minutes;

[0044] b. Mix the wall material, auxiliary wall material and antioxidant in the formula amount in water (the mass ratio of solid to liquid is 1:1.5), stir until uniformly dispersed, and prepare an aqueous phase solution;

[0045] c. Then slowly add the described oil phase solution into the described water phase solution, and obtain an emulsion after high-speed shearing (10000r / min, 2min in total);

[0046] d. The prim...

Embodiment 2

[0050] A lutein microcapsule with strong antioxidative properties, which is prepared from the following components in mass percentage:

[0051] Lutein Crystals 3%

[0052] Sunflower Oil 15%

[0053] Octenyl succinate starch 50%

[0054] Sucrose 31%

[0055] Sodium L-Ascorbate 1%.

[0056] The specific preparation method is as follows:

[0057] a. Put lutein crystals into sunflower oil, mix and stir until uniformly dispersed, and prepare an oil phase solution under the conditions of a melting temperature of 160°C and a melting time of 2 minutes;

[0058] b. Mix the wall material, auxiliary wall material and antioxidant in the formula amount in water (solid-liquid mass ratio is 1:2), stir until uniformly dispersed, and prepare an aqueous phase solution;

[0059] c. Then slowly add the described oil phase solution into the described water phase solution, and obtain an emulsion after high-speed shearing (10000r / min, 2min in total);

[0060] d. The primary emulsion was homoge...

Embodiment 3

[0064] A lutein microcapsule with strong antioxidative properties, which is prepared from the following components in mass percentage:

[0065] Lutein Crystals 5%

[0066] Sunflower Oil 25%

[0067] Gelatin 45%

[0068] Sucrose 24.8%

[0069] Sucrose Stearate 0.1%

[0070] Lecithin 0.1%.

[0071] The specific preparation method is as follows:

[0072] a. Put lutein crystals into sunflower oil, mix and stir until uniformly dispersed, and prepare an oil phase solution under the conditions of a melting temperature of 150°C and a melting time of 2 minutes;

[0073] b. Mix the wall material, auxiliary wall material and antioxidant in the formula amount in water (the mass ratio of solid to liquid is 1:1.5), stir until uniformly dispersed, and prepare an aqueous phase solution;

[0074] c. Then slowly add the oil phase solution into the water phase solution, high-speed shear (10000r / min, total treatment 2min) to prepare the emulsion;

[0075] d. The primary emulsion was homogene...

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Abstract

The invention discloses high-inoxidizability lutein microcapsules.The microcapsules are prepared from a core material, a wall material, an auxiliary material and an antioxidant, the core material is a combination of lutein crystals and sunflower seed oil, the wall material is one of or a mixture of starch sodium octenyl succinate, gelatin and Arabic gum, the auxiliary wall material is one of or a mixture of sucrose stearate, sodium caseinate, lactose and sucrose, the antioxidant is one of or a mixture of L-ascorbyl palmitate, L-sodium ascorbate and lecithin, and a mass ratio of the core material, the wall material, the auxiliary wall material and the antioxidant is 5-30:20-60:10-40:0.3-3.The invention further discloses a preparation method of the microcapsules.Spray granulation and cold air boiling drying technologies are improved, and yield of the microcapsules is obviously increased while waste of raw materials is reduced.By using the preparation method, oxidization stability of the lutein microcapsules can be improved greatly, so that shelf life of the microcapsules is prolonged.

Description

technical field [0001] The invention relates to a preparation and a preparation method thereof, belonging to the technical field of pharmaceutical preparations. Background technique [0002] Lutein, also known as "plant lutein", is an oxygen-containing carotenoid without vitamin A activity, which is widely found in plants such as bananas, kiwis, corns and marigolds. Lutein is a natural coloring agent, which has the advantages of bright color, strong coloring power, safety and non-toxicity. At the same time, lutein has obvious biological effects such as anti-oxidation, anti-aging and anti-mutation. In particular, it shows a strong effect on vision protection, and can prevent macular degeneration and senile cataract. Lutein has been widely used in food, health products, medicine, animal feed and other fields. [0003] However, due to the conjugated polyene structure of lutein, its chemical stability is poor, and it is easily degraded by oxygen, light, temperature, etc., mak...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K9/50A61K31/047A61P27/02A61P27/12A61P39/06B01J13/04A23L33/105A23P10/30A23K10/30A23K20/10
CPCA61K9/5015A61K9/5036A61K9/5057A61K31/047A61K47/14A61K47/24B01J13/04
Inventor 唐俊沈雷花卫俊
Owner 江苏九如食品有限公司
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