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A method for preparing an artificial core and an artificial core prepared by the method

A technology for artificial cores and cores, applied in the field of petroleum exploration, can solve the problems of influence and support and decrease of the overall strength of the cores, so as to reduce the interference factors, facilitate the influence mechanism, and overcome the insufficient strength of the cores.

Active Publication Date: 2018-11-09
CHINA PETROLEUM & CHEM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When this type of method is used to prepare high-permeability cores, the overall strength of the core will be greatly reduced because the contact surface between the matrix material and the bonding material is too small. When the problem is serious, it will affect experimental operations such as support

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0028] The invention provides a kind of preparation method of artificial rock core, comprises the steps:

[0029] (1) Prepare the adhesive.

[0030] In a specific embodiment, cement slurry is used as the adhesive. Specifically, water and cement are mixed, fully stirred evenly, and a cement slurry with a water content of 30-35wt% (preferably 32-35wt%) is prepared. The cement slurry with a moisture content of 30-35wt%, especially the cement slurry with a moisture content of 32-35wt%, can be thoroughly wetted to ensure normal curing, while ensuring that the cement slurry cannot flow or has poor fluidity to prevent excessive Water affects decomposable materials.

[0031] (2) Prepare a decomposable material wrapped with an oil-soluble viscous liquid film.

[0032] Mix the decomposable material with the oil-soluble viscous liquid, and stir well so that the surface of the decomposable material is covered with the oil-soluble viscous liquid. The amount of oil-soluble viscous liqui...

Embodiment 1

[0049] (1) Mix water and cement (general-purpose cement), fully stir evenly, make the cement slurry that water content is 35wt%, get 60 grams for subsequent use.

[0050] (2) 30 grams of ammonium carbonate are mixed with excess liquid paraffin, fully stirred, ammonium carbonate surface is covered by liquid paraffin, remove unnecessary liquid paraffin by decompression suction filtration, thereby obtain the ammonium carbonate that has wrapped liquid paraffin.

[0051] (3) 60 grams of cement slurry of step (2) is mixed with the ammonium carbonate wrapped in liquid paraffin of step (2), and stirred quickly for 2 minutes at a speed of 200rpm, so that the ammonium carbonate wrapped in liquid paraffin is uniformly distributed in the cement slurry , a mixture of the two is obtained.

[0052](4) Add the above mixture into the mold, control the pressure environment to 10MPa, continue for 24 hours, and take out the prepared rock core to be decomposed from the mold.

[0053] (5) The core...

Embodiment 2

[0055] (1) Mix water and cement, fully stir evenly, make the cement slurry that water content is 30wt%, get 75 grams for subsequent use.

[0056] (2) 20 grams of ammonium bicarbonate are mixed with excess pitch, fully stirred, the ammonium bicarbonate surface is covered by pitch, and excess pitch is removed by decompression suction filtration, thereby obtaining ammonium bicarbonate wrapped in pitch.

[0057] (3) 75 grams of cement slurry of step (2) is mixed with the ammonium bicarbonate wrapped in asphalt of step (2), and stirred quickly for 1 minute at a speed of 400rpm, so that the ammonium bicarbonate wrapped in asphalt is evenly distributed in the cement slurry , a mixture of the two is obtained.

[0058] (4) Add the above mixture into the mold, control the pressure environment to 15MPa, continue for 24 hours, and take out the prepared rock core to be decomposed from the mold.

[0059] (5) The core to be decomposed was placed in an environment of 100° C. for 1 hour, and ...

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Abstract

The invention provides a method for preparing an artificial rock core, wherein the method includes the steps: (1) preparing an adhesive; (2) fully mixing a decomposable material and an oil soluble viscous liquid, to make the surface of the decomposable material surface covered with the oil soluble viscous liquid, then removing the excess oil soluble viscous liquid, and thus obtaining a decomposable material wrapped with an oil soluble viscous liquid film; (3) fully mixing evenly the decomposable material wrapped with the oil soluble viscous liquid film with an adhesive to obtain a mixture; (4) placing the mixture obtained in the step (3) in a mold, and carrying out pressurization molding to obtain a to-be-decomposed rock core; and (5) heating the to-be-decomposed rock core obtained in the step (4), fully decomposing the decomposable material, and thus obtaining the artificial rock core. The invention also provides the artificial rock core prepared by the method; the permeability is 600-800 mD, and the strength is 15-20 MPa.

Description

technical field [0001] The invention relates to the field of petroleum exploration, in particular to a method for preparing a high-permeability artificial rock core and the obtained artificial rock core. Background technique [0002] Rock core is an important material for studying the influence of chemical substances on formations. The cost of obtaining natural rock cores is high, and the important parameter of rock cores—permeability—is difficult to control due to different rock collection locations. Therefore, the manufacture of artificial cores with different permeability has important implications for the study of oilfield chemicals. [0003] The preparation of artificial cores is essentially to bond the matrix materials together with adhesives. The matrix material is usually a material with a relatively uniform particle size such as quartz sand and ceramsite. Adhesives are curable molding materials such as epoxy resins, cement, and the like. Permeability arises throu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N1/28C04B38/02C04B28/00
CPCC04B28/00C04B38/02C04B2201/50G01N1/28C04B22/10C04B24/36
Inventor 张雄耿宇迪赵兵陈定斌罗攀登张俊江宋志峰方裕燕李楠秦飞侯帆杨晓武焦克波
Owner CHINA PETROLEUM & CHEM CORP