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Composite fast-hardening silicate leakage stopping slurry and leakage stopping method thereof

A plugging method and silicate technology, applied in the field of oil drilling, can solve the problems of insufficient rigidity strength of concrete curing, large cracks or extra-large malignant ineffectiveness, insufficient rigidity strength of gel plugging, and overcome the initial setting. The effect of long time, reducing the missed recurrence rate, and good market application prospects

Inactive Publication Date: 2016-11-23
中国石油集团川庆钻探工程有限公司长庆钻井总公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The buried depth of the Jurassic Luohe Formation in Changqing Xifeng Oilfield is 700-1100m, the underground temperature is between 28-35°C, and vertical and horizontal fractures are developed. The water is relatively active, and conventional bridge plugging, cement slurry plugging, etc. are easily diluted and dissolved by formation water, and the plugging effect is poor, time-consuming and material-consuming, affecting the construction progress, and the one-time success rate of plugging is less than 50%. :
[0003] 1. The rigidity of the plugging material is insufficient
[0004] All the bridge plugging materials currently used cannot reach the solidified rigidity of concrete, and are almost ineffective for large cracks or extra-large malignancies;
[0005] 2. Existing plugging materials lack adhesion to rocks and have insufficient hydraulic erosion resistance
[0007] 3. Insufficient rigidity and strength of gel plugging
[0008] Although chemical gel has many advantages, such as: better pumpability, delayed crosslinking, late gelation, water repellency, rock adhesion, overall tensile capacity (tension) and compressive capacity (elasticity), etc., but the lack of congenital composition (solid content <10%) restricts the performance of its overall comprehensive rigidity;
[0009] 4. Defects of cement injection plugging process
[0011] ②The cured cement plug layer has only rigid strength, and lacks "flexibility" under the action of mechanical stress, and may be fractured again by the exciting pressure of the drilling fluid in the wellbore

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] In order to solve the above technical problems, this embodiment provides a composite quick-setting silicate plugging that is suitable for the treatment of fractured leakage in the Luohe Formation in the Longdong block, as well as any large-scale leakage with a formation temperature between 30°C and 50°C. The leakage slurry and its plugging method, the silicate plugging slurry includes a main agent and a curing agent, the volume ratio of the main agent and the curing agent is 5:1, and the two are mixed to form a solid gel.

[0030] This composite quick-setting silicate plugging method of the present invention comprises the following steps:

[0031] Step 1) Determine the amount of plugging slurry according to the height of the static liquid level in the wellbore after the leakage layer is lost;

[0032] Step 2) Drill the bare drill pipe down to 5-10m to the top of the leaking layer, dig a plugging pit under the drill floor, cover it with anti-seepage cloth, run it into th...

Embodiment 2

[0042] This embodiment provides a composite quick-setting silicate plugging slurry, including a main agent and a curing agent, the volume ratio of the main agent and the curing agent is 5:1, and the two are mixed to form a solid gel under alkaline conditions.

[0043] The main agent is sodium polysilicate, and the pH value of sodium polysilicate is 12, that is, alkaline. The curing agent is a mixture of ethyl acetate and n-butyl acetate with a mass ratio of 1:1, which has delayed release, timing Gel function, the main agent and the curing agent are mixed to form a solid gel under alkaline conditions. Sodium polysilicate, ethyl acetate and n-butyl acetate can be purchased directly from the market.

[0044] The composite quick-setting silicate plugging slurry of the present invention realizes the organic combination of two systems of organic matter and cement, has a high bulk density, improves its compressive strength, and overcomes the defect of long initial setting time of the...

Embodiment 3

[0046] This example provides a composite quick-setting silicate plugging slurry and its plugging method. The new composite quick-setting silicate plugging technology was used to test two wells in Xifeng Oilfield, as follows:

[0047] Well Ban 56-43 was drilled to 690 meters and the mud suddenly lost its return, and the static liquid level was 80 meters when the drill was pulled out. 6 cubic meters of composite silicate plugging slurry was used for plugging. The volume ratio of the main agent and the curing agent is 5:1, and the two are mixed to form a solid gel under alkaline conditions. glue.

[0048]Well Zhen 302-806 was drilled to 1350 meters of mud return, and the static liquid level was 160 meters when the drill was pulled out. 6 cubic meters of composite silicate plugging slurry was used for plugging. After the plugging was completed, the leaking layer was drilled and lost again. Continue to try 12 cubic meters of composite silicate plugging slurry. After the plugging i...

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Abstract

The invention provides composite fast-hardening silicate leakage stopping slurry and a leakage stopping method thereof. The silicate leakage stopping slurry comprises a main agent and a curing agent, a volume ratio of the main agent to the curing agent is 5:1, and the main agent and the curing agent are mixed to form solid gel. Industrial sodium silicate serving as the main agent and organic ester serving as the gel delay curing agent to form the solid gel under an alkaline condition to realize leakage stopping, water repellency of a leakage stopping system is improved, strength of a leakage stopping layer is improved, mixed alternation of formation water and the leakage stopping slurry can be effectively inhibited, gradual enhancement along with time after injection of the slurry into a leak layer is kept, pressure bearing capacity of the leak layer is improved, the problem of leakage of loss return type absorption wells is solved, one-time leakage stopping success rate is increased and exceeds 50%.

Description

technical field [0001] The invention relates to the technical field of petroleum drilling, in particular to a composite quick-setting silicate plugging slurry and a plugging method thereof, which are suitable for fractured leakage in the Luohe Formation in the Longdong block. Background technique [0002] The buried depth of the Jurassic Luohe Formation in Changqing Xifeng Oilfield is 700-1100m, the underground temperature is between 28-35°C, and vertical and horizontal fractures are developed. The water is relatively active, and conventional bridge plugging, cement slurry plugging, etc. are easily diluted and dissolved by formation water, and the plugging effect is poor, time-consuming and material-consuming, affecting the construction progress, and the one-time success rate of plugging is less than 50%. : [0003] 1. The rigidity of the plugging material is insufficient [0004] All the bridge plugging materials currently used cannot reach the solidified rigidity of conc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/44E21B33/13
CPCC09K8/44C09K8/426E21B33/13
Inventor 张迁吴付频吴农宣柳伟荣朱明明
Owner 中国石油集团川庆钻探工程有限公司长庆钻井总公司
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