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Preparation method of alcohol ether borate brake fluid

A technology of alcohol ether borate and brake fluid, applied in petroleum industry, base materials, additives, etc., can solve the problems of poor water capacity, easy precipitation of precipitates, sensitivity of borate to water, etc., and achieve high temperature resistance to gas. The effect of strong resistance, good low temperature fluidity and excellent physical and chemical properties

Inactive Publication Date: 2016-12-07
辽宁道博精细化学品生产有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above patents and some borate brake fluids on the market have the following problems to varying degrees: the selected dialkyl ether contains tert-butyl ether or dibutyl ether, poor water capacity, and large rubber expansion , The boric acid ester in the brake fluid is sensitive to water. When storing or absorbing water, it is easy to precipitate sediment, which brings the hidden danger of unsafe braking.

Method used

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  • Preparation method of alcohol ether borate brake fluid
  • Preparation method of alcohol ether borate brake fluid

Examples

Experimental program
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Effect test

Embodiment 1

[0027] at 1.2m 3 In the reconciling kettle, add 360 kilograms of triethylene glycol monomethyl ether borate, 250 kilograms of polyethylene glycol monobutyl ether borate, 200 kilograms of triethylene glycol monomethyl ether, 180 kilograms of diethylene glycol, antioxidant Add 2 kg of agent T501, 1 kg of tolyltriazole, and 7 kg of butylamine ether into the reaction kettle in turn, and stir for 30 minutes at 30°C. After the raw materials are fully dissolved, filter them into the finished product tank.

Embodiment 2

[0029] at 1.2m 3 Add 400 kilograms of triethylene glycol monomethyl ether borate, 200 kilograms of polyethylene glycol monobutyl ether borate, 150 kilograms of triethylene glycol monoethyl ether, and 60 kilograms of triethylene glycol dimethyl ether in the blending kettle. , 180 kilograms of triethylene glycol, 12 kilograms of antioxidant T50, 2 kilograms of benzotriazole, and 6 kilograms of methylpropylamine ether, add the above-mentioned raw materials in the reaction kettle in turn, stir for 60 minutes at 50 ° C, after the raw materials are fully dissolved, filter into finished tanks.

Embodiment 3

[0031] at 1.2m 3 Add 430 kilograms of triethylene glycol monomethyl ether borate, 120 kilograms of polyethylene glycol monobutyl ether borate, 200 kilograms of triethylene glycol monomethyl ether, and 80 kilograms of triethylene glycol dimethyl ether in the blending kettle. kg, 160 kg of PEG-188, 2 kg of bisphenol A, 1 kg of benzotriazole, and 7 kg of butylamine ether, add the above raw materials into the reaction kettle in turn, stir at 80°C for 120 minutes under normal pressure, and the raw materials are fully dissolved After that, it is filtered into the finished tank.

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Abstract

A preparation method of an alcohol ether borate brake fluid comprises the following steps: adding raw materials to a reaction kettle, stirring the raw materials at a temperature from room temperature to 90 DEG C until all the raw materials are fully dissolved, and filtering the obtained mixture to obtain the brake fluid, wherein the raw materials comprise, by weight, 20-50% of triethylene glycol monomethyl ether borate, 10-45% of polyethylene glycol monobutyl ether borate with the number-average molecular weight of 780, 10-40% of polyethylene glycol monoalkyl ether, 10-40% of polyethylene glycol, 0-15% of triethylene glycol dimethyl ether, 0-3% of an antioxidant, 0-5% of a pH regulator and 0-5% of a corrosion inhibitor. The preparation method disclosed in the invention solves the instability problem of common borate brake liquids, and allows the alcohol ether borate brake fluid to have the advantages of strong air blockage resistance, good low-temperature fluidity, rust prevention, corrosion prevention, good adaptability to rubber members, and excellent thermal stability.

Description

technical field [0001] The invention relates to a preparation method of brake fluid, in particular to a preparation method of alcohol ether borate type brake fluid comprising triethylene glycol monomethyl ether borate and polyethylene glycol monobutyl ether borate. Background technique [0002] Automobile brake fluid is commonly known as brake oil. Adding brake fluid to automobile brakes is based on the famous Pascal's principle: when pressure is applied to the liquid, the pressure transmitted by the liquid in all directions is equal. By applying pressure to the brake fluid of the car, the main pump and the slave pump interact to the piston of the brake pump, and then apply it to the brake shoe (caliper) to achieve car braking. With the rapid development of the automobile industry in the past two decades, the technology of automobile braking systems has also been greatly improved. The use of anti-lock brakes (ABS) and four-wheel braking electronic balance stabilization syste...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04C10N30/02C10N30/12C10N30/10C10N40/08
CPCC10M105/78C10M125/20C10M129/14C10M129/16C10M133/06C10M133/44C10M169/04C10N2030/02C10N2030/10C10N2030/12C10N2040/08
Inventor 刘博刘金龙
Owner 辽宁道博精细化学品生产有限公司
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