Anodes for lithium-ion devices
A lithium ion and negative electrode technology, applied in the field of lithium ion devices, can solve the problems of mechanical instability, poor Coulombic efficiency, poor life cycle, etc.
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[0026] Preparation of the negative electrode may include grinding and / or mixing processes. In some embodiments, silicon powder and graphite powder can be inserted into a high energy ball mill for milling under a protective atmosphere or a non-protective atmosphere. In some embodiments, boron carbide (B 4C) The powder is added to the pre-ground Si / C mixture inside the mill. The grinder can include hardened alumina media that can be agitated at 1000-1500 RPM. The milling stage can produce an alloy of nano-sized particles having a particle size of about 20-100 nm. In some embodiments, an emulsion containing nano-sized tungsten carbide (WC) particles can be added to the ground powder (Si / C or SI / C / B alloy) at the end of the milling process to produce the active material for the negative electrode. The tungsten carbide grain size may be about 20 to 60 nm. As used herein, "nano-sized" particles refer to particles having an average particle size of less than 1 micron, in embodime...
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[0033] refer to figure 2 , which shows the first cycle charge-discharge curves of an exemplary Li-ion half-cell for a silicon-based negative electrode comprising boron according to some embodiments of the present invention. The voltage of the half cells is expressed as a function of the charge value in mAh / g. An exemplary negative electrode material includes (by weight percent of the total weight of the negative electrode) 48% C, 30% Si, 5.5% B, 8.3% binder, and 8.2% conductive additive (C 0.48 Si 0.30 B 0.055 Adhesive 0.083 conductive additive 0.082 ). The ground C / Si / B alloy (i.e. the active material) contained 57% by weight of C, 36% of Si and 7% of B (C 0.57 Si 0.36 B 0.07 ). Observed figure 2 The graph of , yielded 792 mAh / g on charge and 760 mAh / g on discharge, giving a first cycle efficiency of 96%. The first cycle efficiency is defined as the first discharge amount divided by the first charge amount. It should be noted that within the discharge curve ther...
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