A kind of preparation method of volatile organic compound waste gas active adsorbent

A technology of organic compounds and active adsorbents, which is applied in the field of preparation of active adsorbents for volatile organic compound waste gas, can solve the problems of high cost, complex process, high energy consumption, etc., achieve long replacement cycle, large adsorption capacity, and reduce environmental pollution Effect

Active Publication Date: 2019-05-03
榆林中科环保科技集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Example 1 of the prior art uses zeolite and activator (catalyst) copper oxide and oxyferric chloride to be calcined in a muffle furnace to prepare an organic waste gas adsorbent, which utilizes the characteristics of large specific surface area and strong adsorption capacity of zeolite. Utilize copper oxide, oxyferric chloride activation to enhance adsorption capacity, usually muffle furnace is used for experimental analysis, and the method description is also an experimental process, that is to say, this technology is still far away from industrialization; Activated carbon is used as the raw material, and it is modified and activated. The final step is to send it into a calciner for calcination and grinding. It is similar to two activated carbon activation processes: first activate the raw material to make activated carbon, and then activate the activated carbon to make an adsorbent. General-purpose activated carbon, the process is more complicated, and twice heating, energy consumption is higher, and the cost is also much higher at the same time; The processing method of circulating fluidized bed boiler fly ash mentioned in prior art example 3 is water or water and water and A mixture of surfactants is used to modify the surface of circulating fluidized bed boiler fly ash to become raw materials such as cement, concrete, brick, ceramsite, fillers, etc., so using it sacrifices its large specific surface area and good adsorption activity. Characteristic while high value utilizes the value of active adsorbents for VOC waste gases

Method used

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  • A kind of preparation method of volatile organic compound waste gas active adsorbent

Examples

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Effect test

Embodiment 1

[0015] This example provides a method for preparing an active adsorbent for volatile organic compound waste gas. The components are calculated by weight: 100 parts of circulating fluidized bed coal-fired boiler fly ash, 5 parts of sulfur, 1 part of disulfur dichloride, Sulfur is heated to 460-480°C to form superheated sulfur vapor, which enters the activation prilling tower at a flow rate of 2-3m / s and is mixed with disulfur dichloride at -20--15°C and the circulating flow sent from the bottom of the tower After the exhaust gas from the fluidized bed waste heat boiler is mixed, it is rapidly cooled to below 90°C to form sulfur glue and disulfide dichloride mist droplets. Glue, disulfur dichloride, and fly ash of circulating fluidized bed coal-fired boiler are fully mixed under the purge of exhaust gas from circulating fluidized bed waste heat boiler and spirally rise in the activated prilling tower. Sulfur gum, disulfur dichloride The mist droplets bond the circulating fluidiz...

Embodiment 2

[0017] This example provides a method for preparing an active adsorbent for waste gas of volatile organic compounds. The components are calculated by weight: 100 parts of circulating fluidized bed coal-fired boiler fly ash, 10 parts of sulfur, 1 part of disulfur dichloride, Sulfur is heated to 460-480°C to form superheated sulfur vapor, which enters the activation prilling tower at a flow rate of 2-3m / s and is mixed with disulfur dichloride at -20--15°C and the circulating flow sent from the bottom of the tower After the exhaust gas from the fluidized bed waste heat boiler is mixed, it is rapidly cooled to below 90°C to form sulfur glue and disulfide dichloride mist droplets. Glue, disulfur dichloride, and fly ash of circulating fluidized bed coal-fired boiler are fully mixed under the purge of exhaust gas from circulating fluidized bed waste heat boiler and spirally rise in the activated prilling tower. Sulfur gum, disulfur dichloride The mist droplets bond the circulating fl...

Embodiment 3

[0019] This example provides a method for preparing an active adsorbent for waste gas of volatile organic compounds. The components are calculated by weight: 100 parts of circulating fluidized bed coal-fired boiler fly ash, 5 parts of sulfur, 1.5 parts of disulfur dichloride, Sulfur is heated to 460-480°C to form superheated sulfur vapor, which enters the activation prilling tower at a flow rate of 2-3m / s and is mixed with disulfur dichloride at -20--15°C and the circulating flow sent from the bottom of the tower After the exhaust gas from the fluidized bed waste heat boiler is mixed, it is rapidly cooled to below 90°C to form sulfur glue and disulfide dichloride mist droplets. Glue, disulfur dichloride, and fly ash of circulating fluidized bed coal-fired boiler are fully mixed under the purge of exhaust gas from circulating fluidized bed waste heat boiler and spirally rise in the activated prilling tower. Sulfur gum, disulfur dichloride The mist droplets bond the circulating ...

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Abstract

The invention relates to the technical field of volatile organic compound waste gas treatment, in particular to a preparation method of a volatile organic compound waste gas activated adsorbent. The preparation method is characterized in that 100 parts of circulating fluidized bed coal-fired boiler fly ash, 5-10 parts of sulfur and 1-1.5 parts of disulfur dichloride are proportioned by weight and are activated and granulated, and boiler tail gas and boiler-discharged pollutants such as smoke dust are utilized in a high-value mode to prepare the VOCs adsorbent, and the purposes of providing the cheap VOCs adsorbent, saving energy, reducing emissions, recycling resources and the like are achieved.

Description

technical field [0001] The invention relates to the technical field of waste gas treatment of volatile organic compounds, in particular to a method for preparing an active adsorbent for waste gas of volatile organic compounds. Background technique [0002] Gaseous pollutants emitted by industry are the main source of atmospheric environmental pollutants, among which volatile organic compound waste gas (VOCs) is a gaseous pollutant that is seriously harmful to the environment, and it is also an occupational hazard that affects the health of operators in the workplace It is widely derived from chemical industries such as paints, coatings, coatings, lubricants, and rubber. Due to its huge destructive effect on the human body and the natural environment, the country has issued relevant laws and regulations to strictly control its governance and emissions. At present, the commonly used treatment methods of organic waste gas treatment technology include combustion method, chemica...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/20B01J20/30B01D53/02
CPCB01D53/02B01D2257/708B01J20/20B01J2220/4887Y02A50/20
Inventor 杨松
Owner 榆林中科环保科技集团有限公司
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