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A preparation method of high-precision and extremely small-sized self-supporting beryllium thin film

A high-precision, beryllium-supporting technology, which is applied in vacuum evaporation plating, coating, sputtering plating, etc. Support the problem of low applicability of beryllium film, and achieve the effect of regular shape, high quality and smooth surface

Active Publication Date: 2019-05-28
LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

High-precision and extremely small-sized self-supporting beryllium films are often used as state equation targets in laser physics experiments, X-ray filters on some precision instruments, etc. The target or filter has extremely high requirements for the dimension accuracy of self-supporting beryllium films. Conventional self-supporting film preparation methods cannot meet the requirements
[0004] At present, the preparation method of large-scale self-supporting beryllium film has been reported. Generally, a mask of a certain size is used as the shape of the self-supporting beryllium film. The dimensional accuracy of the mask is generally not high. effect, which eventually leads to a difference between the size of the self-supporting beryllium film and the size of the mask. This method is less applicable to the preparation of high-precision and extremely small self-supporting beryllium films

Method used

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  • A preparation method of high-precision and extremely small-sized self-supporting beryllium thin film
  • A preparation method of high-precision and extremely small-sized self-supporting beryllium thin film
  • A preparation method of high-precision and extremely small-sized self-supporting beryllium thin film

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Embodiment

[0030] A method for preparing a self-supporting beryllium thin film with high precision and extremely small size, comprising the following steps in sequence:

[0031] Step 1: Precision CNC machining of high-precision steps on the surface of the copper block

[0032] In this embodiment, a pure copper block of 10mm×10mm×10mm is used as the substrate (the inventor has proved through experiments that the present invention can be realized in any size of 10mm×10mm×10mm~15mm×15mm×15mm), and an appropriate clamping method, Cutting tool and chip parameters, etc., are milled in layers on the surface of the copper block to produce high-precision steps with a step height of 1mm~2mm. Due to the high precision of the CNC machining method, generally up to 1 μm, the shape (circular or square) of the steps can be precisely controlled to a certain value between tens of μm and hundreds of μm by using this processing method. The outer dimension of the step is the outer dimension of the high-prec...

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Abstract

The invention discloses a preparing method of a high-precision self-supporting beryllium film with the minimum size. The preparing method sequentially comprises the following steps that a high-precision step is machined on the surface of a copper block body; the roughness of the end face of the copper step is meticulously grinded to the nanometer magnitude level; an aluminum film is evaporated and deposited on the end face of the copper step; the beryllium film is deposited on the surface of the aluminum film; a NaOH solution reaction is adopted for removing a substrate of the aluminum film, and the high-precision self-supporting beryllium film with the minimum size is obtained. The method greatly improves the size precision of the high-precision self-supporting beryllium film with the minimum size, and precision can reach 1 micrometers. Moreover, the obtained self-supporting beryllium film is smooth in surface, free of sand holes, regular in shape and excellent in quality.

Description

technical field [0001] The invention relates to the technical field of self-supporting beryllium thin films, more specifically, the invention relates to a preparation method of high-precision and extremely small-sized self-supporting beryllium thin films. Background technique [0002] Beryllium (Be) is one of the rare metals. Compared with other low-sequence metal materials, it has low density, high melting point, high strength and elastic modulus, large specific heat capacity, high X-ray transmittance, and adjustable thermal neutron scattering. And other characteristics, its unique physical and chemical properties make it have important application value in the nuclear industry, aerospace, metallurgical industry and high-tech fields. [0003] A self-supporting beryllium film refers to a beryllium film that exists independently without substrate support. The "high-precision and extremely small-sized self-supporting beryllium film" of the present invention, unless otherwise s...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/02C23C14/16C23C14/24B24B1/00
CPCB24B1/00C23C14/0005C23C14/028C23C14/16C23C14/24
Inventor 李恺吴卫东罗炳池罗江山张吉强谭秀兰李文琦金雷何玉丹
Owner LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS
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