A cuprous oxide-based heterojunction photocathode and its preparation method
A cuprous oxide-based, cuprous oxide technology is applied in the plating and coating of electrodes and superimposed layers, which can solve the problems of too thick, fragile cuprous oxide films, and inconvenient assembly steps, and improve the film quality. , low cost, rich storage effect
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[0041] Preparation of cuprous oxide-based heterojunction photocathode, the structure is as follows figure 1 As shown, it includes the following steps: 1) Put a copper sheet with a purity of 99.99% and a thickness of 100 μm in a corundum crucible, and oxidize it into a cuprous oxide sheet in a tube furnace. The specific steps are:
[0042] a) Put the copper sheet in the tube furnace, pump out the air, and pass in the argon gas to keep the argon atmosphere.
[0043] Raise the temperature to 1050°C at a rate of 15°C / min, and keep it warm for one hour.
[0044] b) At a temperature of 1050°C, air is introduced and the temperature is kept for one hour.
[0045] c) At a temperature of 1050°C, the air is pumped out again, and argon gas is introduced, under the protection of argon gas
[0046] Keep warm for two hours.
[0047] d) Under argon protection, cool down to 500°C at 10°C / min, and then cool naturally to
[0048] Remove from room temperature.
[0049] 2) The above-mentione...
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