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Annealing process for reducing residual magnetism of nanocrystalline magnetic core

An annealing process and nanocrystalline technology, applied in the direction of magnetic core manufacturing, process efficiency improvement, magnetic materials, etc., can solve the problems of limited application, miniaturization of electronic components with low disadvantage, high coercivity, and achieve excellent comprehensive performance, The effect of increasing the first crystallization temperature and low coercivity

Active Publication Date: 2017-11-14
DONGGUAN DAZHONG ELECTRONICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The relatively high coercive force of traditional metal soft magnetic materials limits its application in the soft magnetic field; soft magnetic ferrite is not conducive to the miniaturization of electronic components due to its low saturation magnetic induction; and nanocrystalline alloy soft magnetic materials As an emerging material in this field, it has attracted the attention of many researchers because of its high saturation magnetic induction, high permeability, low loss (much lower than silicon steel), high resistivity and high strength and toughness. It has been put into production and application in the early stage, and its preparation process is simple, energy-saving and environmentally friendly, and it has partially replaced traditional silicon steel and ferrite materials in a few fields

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] A kind of annealing process that reduces the remanence of nanocrystalline magnetic core, comprises the steps:

[0056] (1) Winding the nanocrystalline ribbon into an annular nanocrystalline magnetic core;

[0057] (2) Put the nanocrystalline magnetic core into the vacuum annealing furnace for heat treatment;

[0058] (3) Put the heat-treated nanocrystalline magnetic core into a vacuum annealing furnace for heat treatment again.

[0059] In the step (1), the thickness of the nanocrystalline ribbon is 15 μm, and the width is 20 mm.

[0060] In the step (1), the nanocrystalline ribbon is an iron-based nanocrystalline ribbon, and the iron-based nanocrystalline ribbon includes the following elements by weight percentage: Si: 14%, B: 7%, Nb: 1%, Cu: 1.6%, Zr: 4%, Al: 0.5%, and the balance is Fe.

[0061] The iron-based nanocrystalline ribbon also includes Ga: 0.4%, V: 0.1%, Ti: 0.2, Mn: 1%, Cr: 0.5%, Mo: 0.8%, C: 1.2%, Ge: 0.01%, P : 0.001%, Vb: 1.4%, Ta: 0.3%, and W: 0.0...

Embodiment 2

[0077] A kind of annealing process that reduces the remanence of nanocrystalline magnetic core, comprises the steps:

[0078] (1) Winding the nanocrystalline ribbon into an annular nanocrystalline magnetic core;

[0079] (2) Put the nanocrystalline magnetic core into the vacuum annealing furnace for heat treatment;

[0080] (3) Put the heat-treated nanocrystalline magnetic core into a vacuum annealing furnace for heat treatment again.

[0081] In the step (1), the nanocrystalline ribbon has a thickness of 18 μm and a width of 22 mm.

[0082] In the step (1), the nanocrystalline ribbon is an iron-based nanocrystalline ribbon, and the iron-based nanocrystalline ribbon includes the following elements by weight percentage: Si: 14.5%, B: 7.5%, Nb: 1.5%, Cu: 1.65%, Zr: 4.5%, Al: 0.8%, and the balance is Fe.

[0083] The iron-based nanocrystalline ribbon also includes Ga: 0.5%, V: 0.2%, Ti: 0.3%, Mn: 1.5%, Cr: 0.8%, Mo: 0.9%, C: 1.25%, Ge: 0.02%, P: 0.002%, Vb: 1.5%, Ta: 0.4%, an...

Embodiment 3

[0099] A kind of annealing process that reduces the remanence of nanocrystalline magnetic core, comprises the steps:

[0100] (1) Winding the nanocrystalline ribbon into an annular nanocrystalline magnetic core;

[0101] (2) Put the nanocrystalline magnetic core into the vacuum annealing furnace for heat treatment;

[0102] (3) Put the heat-treated nanocrystalline magnetic core into a vacuum annealing furnace for heat treatment again.

[0103] In the step (1), the nanocrystalline ribbon has a thickness of 20 μm and a width of 25 mm.

[0104] In the step (1), the nanocrystalline ribbon is an iron-based nanocrystalline ribbon, and the iron-based nanocrystalline ribbon includes the following elements by weight percentage: Si: 15%, B: 8%, Nb: 2%, Cu: 1.7%, Zr: 5%, Al: 1.0%, and the balance is Fe.

[0105] The iron-based nanocrystalline ribbon also includes Ga: 0.6%, V: 0.3%, Ti: 0.4%, Mn: 2%, Cr: 1.0%, Mo: 1.0%, C: 1.3%, Ge: 0.03%, P: 0.003%, Vb: 1.6%, Ta: 0.5%, and W: 0.06%. ...

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Abstract

The invention relates to the technical field of high-frequency inverter power supplies, in particular to an annealing process for reducing residual magnetism of a nanocrystalline magnetic core. The annealing process comprises the following steps of (1), winding a nanocrystalline strip into the annular nanocrystalline magnetic core; (2), putting the nanocrystalline magnetic core into a vacuum annealing furnace for a heat treatment; and (3), putting the nanocrystalline magnetic core subjected to the heat treatment into the vacuum annealing furnace for the heat treatment again. According to the annealing process, the nanocrystalline magnetic core which is to undergo the heat treatment undergoes the same heat treatment process twice through the conventional annealing furnace so as to meet the electrical requirement that the transverse magnetic furnace reduces the residual magnetism of the nanocrystalline magnetic core, so that the heat treatment process is simplified, the process is simple, the investment of production equipment is reduced, the power cost can be saved by more than 25%, and the production cost is low; and the nanocrystalline magnetic core prepared by the annealing process has stable magnetic conductivity and direct current bias capability, also has the advantages of high saturation magnetic induction intensity, low loss value, low coercive force, high temperature resistance and the like, and is excellent in comprehensive performance.

Description

technical field [0001] The invention relates to the technical field of high-frequency inverter power supplies, in particular to an annealing process for reducing the remanence of a nanocrystalline magnetic core. Background technique [0002] Soft magnetic materials have magnetic properties such as low coercive force and high magnetic permeability. They are the raw materials for making magnetic cores such as inductors, choke coils, and sensors. They have been widely used in industries such as electric power, motors, and electronics. So far, soft magnetic materials for engineering applications have been divided into metal soft magnetic materials (such as industrial pure iron, silicon steel, permalloy), soft magnetic ferrite, non Crystalline and nanocrystalline soft magnetic materials. The relatively high coercive force of traditional metal soft magnetic materials limits its application in the soft magnetic field; soft magnetic ferrite is not conducive to the miniaturization o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C21D1/26C21D6/00C21D9/00H01F1/147H01F41/02C22C38/02C22C38/04C22C38/06C22C38/12C22C38/16C22C38/20C22C38/22C22C38/24C22C38/26C22C38/28C22C38/32C22C38/34C22C38/38
CPCC21D1/26C21D6/002C21D6/005C21D6/008C21D9/0068C22C38/002C22C38/02C22C38/04C22C38/06C22C38/12C22C38/16C22C38/20C22C38/22C22C38/24C22C38/26C22C38/28C22C38/32C22C38/34C22C38/38H01F1/14775H01F41/0213Y02P10/20
Inventor 梁文超李正中李经伟
Owner DONGGUAN DAZHONG ELECTRONICS