Propylene copolymer composition with improved long-term mechanical properties
A technology of propylene copolymer and ethylene copolymerization, which is applied in the field of thin-walled plastic containers and injection molding products, and can solve the problems of reducing toughness and increasing modulus
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[0278] Preparation of solid catalyst components
[0279] 20.3kg of TiCl 4 and 1.1 kg of toluene were added to a 20 liter stainless steel reactor. With mixing at 350 rpm and keeping the temperature at 0° C., 14.5 kg of the magnesium alkoxide complex prepared in Example 1 were added within 1.5 hours. Add 1.7 liters of 1-254 and 7.5 kg of heptane, and after mixing for 1 hour at 0°C, the temperature of the formed emulsion was raised to 90°C within 1 hour. Mixing was stopped after 30 minutes, the catalyst droplets were allowed to solidify and the formed catalyst particles were allowed to settle. After settling (1 hour), the supernatant was siphoned off.
[0280] The catalyst particles were then washed with 45 kg of toluene at 90° C. for 20 minutes, followed by two heptane washes (30 kg, 15 min). During the first heptane wash, the temperature was lowered to 50°C, and to room temperature during the second wash.
[0281] The solid catalyst component was used together with tri...
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