Polymer coating material with corrosion detection and self-repair functions and preparation method
A polymer coating and corrosion detection technology, applied in the direction of analysis of materials, anti-corrosion coatings, coatings, etc., to achieve the effect of self-detection and self-repair, and prolong service life
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[0028] The preparation method of above-mentioned polymer coating material of the present invention, comprises the following steps:
[0029] Step 1, dissolving the fluorescence detection reagent or self-repair reagent, then adding polymer microcapsules, vacuum impregnating and drying, to obtain polymer microcapsules loaded with fluorescence detection reagent or self-repair reagent;
[0030] Step 2, compounding the polymer microcapsules loaded with the fluorescence detection reagent and the self-repairing reagent into the polymer resin to obtain the polymer coating material.
[0031] In the present invention, the component that develops the color is the fluorescent detection reagent, and the self-repairing anti-corrosion function is the self-repairing reagent. It is only necessary to ensure that the content of the converted fluorescent detection reagent or self-repairing reagent in the polymer coating is not low Therefore, the present invention does not limit the amount of polym...
Embodiment 1
[0039] The fluorescent detection reagent coumarin and the self-repairing reagent benzotriazole were dissolved, then the hollow polystyrene microspheres were added, vacuum impregnated for a period of time and then dried to obtain the hollow polystyrene microspheres loaded with the fluorescent detection reagent and the self-repairing reagent. ball. Hollow polystyrene microspheres loaded with fluorescent detection reagents and self-repairing reagents were dispersed into epoxy resin to obtain an epoxy resin coating material capable of self-detection and self-repairing of corrosion, in which the fluorescence detection reagent coumarin The content is 100ppm, and the content of the self-healing agent benzotriazole is 5000ppm. The resin was applied to the surface of carbon steel to solidify, then immersed in 3.5% NaCl solution, and the corrosion of the surface of carbon steel was detected by laser confocal. At the same time, the carbon steel coated with smart coating and pure epoxy r...
Embodiment 2
[0041] The fluorescent detection reagent coumarin and the self-repairing reagent benzotriazole were dissolved, then the hollow polystyrene microspheres were added, vacuum impregnated for a period of time and then dried to obtain the hollow polystyrene microspheres loaded with the fluorescent detection reagent and the self-repairing reagent. ball. Hollow polystyrene microspheres loaded with fluorescent detection reagents and self-repairing reagents were dispersed into epoxy resin to obtain an epoxy resin coating material capable of self-detection and self-repairing of corrosion, in which the fluorescence detection reagent coumarin The content is 5ppm, and the content of the self-healing reagent benzotriazole is 5ppm. The resin was coated on the aluminum surface to solidify, then immersed in 3.5% NaCl solution, and the corrosion of the aluminum surface was detected by laser confocal. At the same time, aluminum coated with smart coating and pure epoxy resin were simultaneously i...
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