A kind of mo-si-c alloy rod and preparation method thereof
An alloy rod, mo-si-c technology, applied in the field of Mo-Si-C alloy rod and its preparation, can solve the problems of poor high temperature strength, loss of function, limited prospects, etc., to achieve high hardness, low density, The effect of lowering the sintering temperature
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Embodiment 1
[0025] The Mo-Si-C alloy rod in this embodiment is made of the following atomic percentages of raw materials: 20% silicon, 25% carbon, and the balance is molybdenum and unavoidable impurities.
[0026] The method for preparing Mo-Si-C alloy rods in this embodiment comprises the following steps:
[0027] Step 1. Put silicon powder, carbon powder and molybdenum powder in a ball mill, use absolute ethanol as a dispersant, and ball mill for 30 hours at a speed of 300r / min and a ball-to-material ratio of 10:1 by mass. Finally, dry it under vacuum conditions at 85°C to obtain mixed powder; the volume of the absolute ethanol is twice the sum of the mass of silicon powder, carbon powder and molybdenum powder, and the unit of the volume of absolute ethanol is mL. Silicon powder, carbon powder The unit of the total mass of powder and molybdenum powder is g; the mass purity of the silicon powder is not less than 99.5%, the mass purity of the carbon powder is not less than 99.5%, and the ...
Embodiment 2
[0033] The Mo-Si-C alloy rod in this embodiment is made of the following atomic percentages of raw materials: 25% silicon, 35% carbon, and the balance is molybdenum and unavoidable impurities.
[0034] The method for preparing Mo-Si-C alloy rods in this embodiment comprises the following steps:
[0035] Step 1. Put silicon powder, carbon powder and molybdenum powder in a ball mill, use absolute ethanol as a dispersant, and ball mill for 40 hours at a speed of 400r / min and a ball-to-material ratio of 15:1 by mass. Finally, dry under vacuum conditions at 90°C to obtain mixed powder; the volume of the absolute ethanol is 3 times the total mass of silicon powder, carbon powder and molybdenum powder, and the unit of the volume of absolute ethanol is mL, silicon powder, carbon powder The unit of the total mass of powder and molybdenum powder is g; the mass purity of the silicon powder is not less than 99.5%, the mass purity of the carbon powder is not less than 99.5%, and the mass p...
Embodiment 3
[0041] The Mo-Si-C alloy rod in this embodiment is made of the following atomic percentages of raw materials: 15% silicon, 15% carbon, and the balance is molybdenum and unavoidable impurities.
[0042] The method for preparing Mo-Si-C alloy rods in this embodiment comprises the following steps:
[0043] Step 1. Put silicon powder, carbon powder and molybdenum powder in a ball mill, use absolute ethanol as a dispersant, and ball mill for 20 hours at a speed of 200r / min and a ball-to-material ratio of 5:1 by mass ratio. Finally, dry under vacuum conditions at 80°C to obtain mixed powder; the volume of the absolute ethanol is 1 time of the total mass of silicon powder, carbon powder and molybdenum powder, and the unit of the volume of absolute ethanol is mL. The unit of the total mass of powder and molybdenum powder is g; the mass purity of the silicon powder is not less than 99.5%, the mass purity of the carbon powder is not less than 99.5%, and the mass purity of the molybdenum...
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