Preparation method of high-purity fine-grain pure copper material for charge liners
A high-purity, medicine-shaped mask technology, which is applied in the field of preparation of high-purity fine-grained pure copper materials for medicine-shaped masks, can solve problems such as uneven grain size and many impurity elements, and achieve stable material performance and high material yield. The effect of high rate and high production efficiency
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Embodiment 1
[0031] A preparation method of a high-purity fine-grained pure copper material for a drug-type cover is carried out according to the following steps:
[0032] (1) Preparation of blanks: commercial T2 pure copper rods are used, the size specification is φ120mm, and the average grain size is about 250μm (such as figure 1 ), the content of impurity elements is shown in Table 1. Use sawing to cut the material to a length of 500mm to remove oxides and oil on the surface.
[0033] Table 1 Content of impurity elements in T2 copper rods
[0034] Grade
P
Bi
Sb
As
Fe
Ni
sn
S
0
Pb
Zn
sum
T2
60
40
30
20
50
200
20
40
380
120
40
1000
[0035] (2) Vacuum electron beam melting: use an electron beam melting furnace with a power of 900kw for secondary electron beam melting and purification, the copper crystallizer is φ250mm, and the vacuum degree of the melting chamber is ≥2×10 -3 Pa, the pri...
Embodiment 2
[0044] A preparation method of a high-purity fine-grained pure copper material for a drug-type cover is carried out according to the following steps:
[0045] (1) Preparation of the billet: commercial T3 pure copper rods are used, the size specification is φ90mm, and the average grain size is about 130μm (such as image 3 ), the content of impurity elements is shown in Table 3. Use sawing to cut the material to a length of 800mm to remove oxides and oil stains on the surface.
[0046] Table 3 The content of impurity elements in T3 copper rods (×10 -6 )
[0047]
[0048]
[0049] (2) Vacuum electron beam melting: use an electron beam melting furnace with a power of 900kw for secondary electron beam melting and purification, the copper crystallizer is φ250mm, and the vacuum degree of the melting chamber is ≥2×10 -3 Pa, the primary smelting speed is 80kg / h, the ingot rotating and drawing speed is 2mm / min; the secondary melting speed is 100kg / h, and the ingot rotating and...
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