Drugs that cause neuroinflammation-mediated neuronal damage following HIV infection
A technology of AIDS and drugs, which is applied in the application field of drugs for the prevention and treatment of neuron damage caused by HIV-1 Tat protein, and can solve the problems of limited activity and limited effect of lignan compounds
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Embodiment 1
[0018] Embodiment 1: synthetic embodiment
[0019]
[0020]
[0021] resolve resolution:
[0022] Compounds with similar structures to lignan were obtained according to CN201110439347.X, amantadine was purchased from Sigma Chemical Reagent Company, and others were regular reagents in the laboratory. Dissolve triethylamine in ethyl acetate, add lignan structurally similar compounds and amantadine at a molar ratio of 1:1, add HOBT and DCC in excess molar ratio in turn under stirring conditions, filter to remove the precipitate after the reaction is completed, and the filtrate Concentrate to dryness under reduced pressure, add diethyl ether to extract twice, combine the diethyl ether layers, wash with saturated brine, and dry. Filtrate, concentrate under reduced pressure to remove diethyl ether, and pass the residue through a silica gel column with petroleum ether: ethyl acetate = 1:4 to obtain a white solid which is the target product. MS m / z=471 (M + ) for elemental an...
Embodiment 2
[0025] Embodiment 2: pharmacodynamic experiment
[0026] (1) Main reagents, cells and instruments
[0027] HIV-1Tat protein was purchased from Shenzhen Baiwansen Bio-Trade Co., Ltd. (Prospec, USA). Rat adrenal pheochromoma cell line (PC12) was purchased from Shanghai Institute of Cells, Chinese Academy of Sciences. MTT was purchased from Sigma Company; LDH (lactate dehydrogenase) detection kit was purchased from Nanjing Jiancheng Institute of Bioengineering; Tunel detection kit was purchased from Promega Company of the United States. Inactivated fetal bovine serum was purchased from Hangzhou Sijiqing Bioengineering Materials Co., Ltd.; horse serum, DMEM medium and MEM medium were purchased from Gibco; other reagents were of analytical grade. Microplate reader (USA BIOTEK company); Olympus microscopic imaging system (Olympus,
[0028] FV10); Mcllwain automatic tissue slicer (CAMPDEN, 220-240); oscillating slicer (LR59590, USA).
[0029] PC12 cells are rat adrenal pheochromo...
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