A kind of preparation method of thermal insulation mortar
A thermal insulation mortar and calcination technology, which is applied in the field of mortar, can solve the problems of high water absorption and low strength of thermal insulation mortar, and achieve the effects of low water absorption, high strength and increased strength
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[0020] A preparation method of thermal insulation mortar, the preparation method comprises the steps of:
[0021] (1) Take the waste clay and put it into a calciner for calcination at 1200°C for 50 minutes, collect the calcined particles, put the calcined particles and aluminum ash in a ball mill at a mass ratio of 6:2 to 4, and perform ball milling at 800r / min for 1 hour, collect the ball mill Put the ball mill and 1.3mol / L sodium hydroxide solution into the container at a mass ratio of 1:5, and ultrasonically vibrate, heat to 65°C, and heat for 3h;
[0022] (2) After the heating is over, let it stand overnight, then add calcined particles of 15-20% silica to the container, mix well, put the contents in the container into the reaction kettle, use nitrogen protection, at 80-85°C Preheat under low temperature, add an additive solution with 5-7% silica mass, raise the temperature to 120-150°C, and stir for 4-7 hours;
[0023] (3) After stirring, cool to room temperature, discha...
Embodiment 1
[0027] The additive solution was prepared by mixing sodium dodecylbenzenesulfonate and 0.1mol / L chitosan glacial acetic acid solution at a mass ratio of 1:3.
[0028] The choice of air-entraining agent is abietic acid.
[0029] The choice of hydrophobic agent is N-12.-aminoethyl 3-aminopropyltrimethoxysilane.
[0030] A preparation method of thermal insulation mortar, the preparation method comprises the steps of:
[0031] (1) Take the waste clay and put it into a calciner for calcination at 1200°C for 50 minutes, collect the calcined particles, put the calcined particles and aluminum ash in a ball mill at 800r / min for 1 hour at a mass ratio of 6:4, and collect the ball milled matter. Put the ball mill and 1.3mol / L sodium hydroxide solution into the container at a mass ratio of 1:5, and conduct ultrasonic vibration, heat to 65°C, and heat for 3h;
[0032] (2) After the heating is over, let it stand overnight, then add calcined particles of 20% silica to the container, mix we...
Embodiment 2
[0037] The additive solution was prepared by mixing sodium dodecylbenzenesulfonate and 0.1mol / L chitosan glacial acetic acid solution at a mass ratio of 1:3.
[0038] The choice of air-entraining agent is sodium alkylbenzene sulfonate.
[0039] The choice of hydrophobic agent is N-12.-aminoethyl 3-aminopropyltrimethoxysilane.
[0040] A preparation method of thermal insulation mortar, the preparation method comprises the steps of:
[0041] (1) Take the waste clay and put it into a calciner for calcination at 1200°C for 50 minutes, collect the calcined particles, put the calcined particles and aluminum ash in a ball mill at a mass ratio of 6:3 and perform ball milling at 800r / min for 1 hour, and collect the ball milled matter. Put the ball mill and 1.3mol / L sodium hydroxide solution into the container at a mass ratio of 1:5, and conduct ultrasonic vibration, heat to 65°C, and heat for 3h;
[0042] (2) After the heating is over, let it stand overnight, then add calcined partic...
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