A kind of ultra-high strength thermal insulation material and preparation method thereof
An insulation material and ultra-high-strength technology, applied in the field of new high-strength insulation materials, can solve problems such as low strength and easy peeling, achieve high strength, avoid oxidation and decomposition, and avoid the effects of low internal temperature
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[0027] An embodiment of the present invention provides a method for preparing an ultra-high-strength thermal insulation material, comprising the following steps:
[0028] Step 1, using phenolic resin to impregnate the quartz-type chopped reinforcing fiber mat to obtain a prepreg;
[0029] Specifically, in the embodiment of the present invention, the quartz-based chopped reinforcing fiber mat is preferably one or a combination of chopped glass fiber mat or chopped quartz fiber mat, more preferably a chopped fiber mat with a fiber diameter of 6-9 mm. Glass fiber, to ensure that the insulation material obtained has higher strength; the density of the quartz-like chopped reinforcing fiber mat is preferably 120-180kg / m3, to ensure that the fiber mat has good impregnation performance and ensure that the resin matrix is evenly distributed; The resin mass content is preferably 20%-70%, more preferably 23%-30%;
[0030] Step 2, curing the prepreg in an oxygen-enriched environment to...
Embodiment 1
[0038] Step 1. Preparation of prepreg:
[0039] According to the proportion of resin mass content being 25%, adopting phenolic resin to impregnate chopped non-alkali glass fiber mat with fiber diameter of 6-9mm, the density of said chopped non-alkali glass fiber mat is 150kg / m 3 ;
[0040] Step 2, see figure 1 , each of the multiple prepregs 3 prepared in step 1 is supported by a porous partition 4 (porous plate), and stacked in layers. When stacked, the partitions 4 are overhead through the limit block 2 placed on the platform 5 Position limit, press block 1 on the uppermost partition 4 to form a component to be cured, put the component to be cured into a heating furnace, and raise the temperature to 185°C at a heating rate of 5-6°C / min, Keep warm for 3 hours to obtain the insulation material;
[0041] Step 3. Raise the temperature to 350° C. at a heating rate of 10° C. / min, keep it warm for 2 hours, and cool down to obtain an ultra-high-strength thermal insulation materia...
Embodiment 2
[0044] Step 1. Preparation of prepreg:
[0045] According to the proportion that the resin mass content is 70%, adopt phenolic resin to impregnate the chopped non-alkali glass fiber mat with fiber diameter of 6-9mm, the density of the chopped non-alkali glass fiber mat is 150kg / m 3 ;
[0046] Step 2, see figure 1 , each of the multiple prepregs 3 prepared in step 1 is supported by a porous partition 4 (porous plate), and stacked in layers. When stacked, the partitions 4 are overhead through the limit block 2 placed on the platform 5 Position limit, press block 1 on the uppermost partition 4 to form a component to be cured, put the component to be cured into a heating furnace, and raise the temperature to 185°C at a heating rate of 5-6°C / min, Keep warm for 3 hours to obtain the insulation material;
[0047] Step 3. Raise the temperature to 350° C. at a heating rate of 10° C. / min, keep it warm for 2 hours, and cool down to obtain an ultra-high-strength thermal insulation mate...
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Abstract
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