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A kind of fiber silk electrode material and preparation method thereof

A technology of electrode materials and fiber filaments, which is applied in the field of polymer functional materials preparation, can solve the problems of complex process, restricted popularization, environmental pollution, etc., and achieve the effect of simple process, good catalytic performance and low condition requirements

Inactive Publication Date: 2019-03-19
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Solar energy is inexhaustible, and the development and utilization of solar energy has been greatly improved in recent decades. Based on the first generation of solar cells based on silicon crystals and cadmium telluride and copper indium gallium selenide thin films The main second-generation solar cells have good photoelectric conversion efficiency, but the disadvantages of complex process, high cost, and serious environmental pollution restrict the popularization of the two technologies.

Method used

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  • A kind of fiber silk electrode material and preparation method thereof
  • A kind of fiber silk electrode material and preparation method thereof
  • A kind of fiber silk electrode material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] (1) Pipette 100mL of distilled water into a 250mL beaker, and drop into 3mL of glacial acetic acid solution, stir evenly; in the case of mechanical stirring, slowly add 1g of chitosan powder into the solution, and continue to 150 ~ 1700r min -1 Stir rapidly for 3h, and let stand for 24h to discharge the air bubbles in the slurry to obtain chitosan slurry A;

[0043] (2) Weighing 100 mg of graphite oxide into a 100 mL volumetric flask, and ultrasonicating for 2 h to obtain a uniformly dispersed graphene oxide solution, and obtain solution A;

[0044] (3) Pipette 100mL of the solution A obtained in step (2) into a 250mL beaker, slowly add 1g of sodium alginate powder under the condition of mechanical stirring, stir rapidly for 4h, and let stand for 12h to discharge the air bubbles in the slurry to obtain Graphene / sodium alginate slurry B;

[0045] (4) pipette a drop of slurry A on the surface of the glass plate with a rubber dropper;

[0046] (5) Pipette a drop of slurr...

Embodiment 2

[0051] (1) Pipette 100mL of distilled water into a 250mL beaker, drop into 3mL of glacial acetic acid solution, and stir evenly; under the condition of mechanical stirring, slowly add 5g of tetrabutylammonium bromide to the solution, and continue to use 150~1700r· min -1 Stir rapidly for 4h, and let stand for 18h to discharge the air bubbles in the slurry to obtain tetrabutylammonium bromide slurry A;

[0052] (2) Weigh 200mg of fullerene into a 100mL volumetric flask, and sonicate for 4 hours to obtain a uniformly dispersed fullerene solution, and obtain solution A;

[0053] (3) Pipette 100mL of the solution A obtained in step (2) into a 250mL beaker, slowly add 5g of sodium alginate powder under the condition of mechanical stirring, stir rapidly for 4h, and let stand for 24h to discharge the air bubbles in the slurry to obtain Fullerene / sodium alginate slurry B;

[0054] (4) pipette a drop of slurry A on the surface of the glass plate with a rubber dropper;

[0055] (5) P...

Embodiment 3

[0059] (1) Pipette 100mL of distilled water into a 250mL beaker, drop into 3mL of glacial acetic acid solution, and stir evenly; under the condition of mechanical stirring, slowly add 8g of n-octyltrimethylammonium bromide powder into the solution, and continue to 150~1700 rpm -1 Stir rapidly for 4h, and let stand for 24h to discharge the air bubbles in the slurry to obtain n-octyltrimethylammonium bromide slurry A;

[0060] (2) Weigh 400 mg of multi-walled carbon nanotubes into a 100 mL volumetric flask, and sonicate for 6 hours to obtain a uniformly dispersed multi-walled carbon nanotube solution, and obtain solution A;

[0061] (3) Pipette 100mL of the solution A obtained in step (2) into a 250mL beaker, slowly add 8g of sodium alginate powder under the condition of mechanical stirring, stir rapidly for 4h, and let stand for 24h to discharge the air bubbles in the slurry to obtain Multi-walled carbon nanotubes / sodium alginate slurry B;

[0062] (4) pipette a drop of slurr...

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Abstract

The invention discloses a filament electrode material and a preparation method thereof. The specific preparation method comprises the following steps of (1) mixing and stirring deionized water and a glacial acetic acid solution evenly, adding chitosan powder to a mixed solution, continuing to stir, standing and discharging bubbles in slurry to obtain slurry A; (2) slowly adding sodium alginate powder to an evenly dispersed graphene oxide solution, quickly stirring, standing and discharging the bubbles in the slurry to obtain slurry B; (3) transferring a drop of slurry A for dripping on the surface of a glass plate and transferring a drop of slurry B for dripping next to the slurry A; (4) inserting two tips of precision tweezers into the slurry A and the slurry B separately, and clamping and extracting the slurry A and the slurry B upwards to form a filamentous line; and (5) standing and suspending the filamentous line obtained in the step (4) to obtain the filament electrode material.The prepared material is simple and convenient to prepare and operate, simple in process, high in speed, low in condition requirement and low in cost.

Description

technical field [0001] The invention belongs to the technical field of polymer functionalized material preparation, and in particular relates to a fiber wire electrode material and a preparation method thereof. Background technique [0002] With the increasing energy crisis and environmental pollution, exploring and developing new environmentally friendly and efficient energy sources is an inevitable choice for the sustainable development of human society. Solar energy is inexhaustible, and the development and utilization of solar energy has been greatly improved in recent decades, based on the first generation of solar cells based on silicon crystals and cadmium telluride and copper indium gallium selenide thin films The main second-generation solar cells have good photoelectric conversion efficiency, but the disadvantages of complex process, high cost, and serious environmental pollution restrict the popularization of the two technologies. Dye-Sensitized Solar Cells (DSSC...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01G9/20H01G9/042H01G9/048
CPCH01G9/2022H01G9/2045Y02E10/542
Inventor 于飞石岩王成显姚温浩陈德贤张方倪腾飞韩生张海英
Owner SHANGHAI INST OF TECH
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