Self-luminous photosensitive resin composition, color filter including color conversion layer using same, and image display device
A photosensitive resin, self-luminous technology, used in luminescent materials, chemical instruments and methods, photosensitive materials for optomechanical equipment, etc., can solve problems such as difficult to expect light efficiency, brightness reduction, etc.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
manufacture example 1
[0157] Production Example 1: Synthesis of Intermediate Compound (INT)
[0158]
[0159] 1,6,7,12-Tetrachloroperylenetetracarboxylic dianhydride (0.11 mol) and 2,6-diisopropylaniline (0.44 mol) were put into 1 L of propionic acid, heated up, and the reaction was maintained at 140°C 5 hours. The reaction solution was cooled to room temperature, and the precipitate was filtered under reduced pressure and washed with methanol and water. The filtrate was dispersed in water, maintained for 30 minutes, filtered under reduced pressure, dispersed in methanol again, maintained for 30 minutes, and then filtered under reduced pressure. After drying, the intermediate compound (INT) was obtained in a yield of 80.5%.
[0160] About the obtained intermediate compound, MS (mass spectrometry) was measured using a MALDI-TOF measuring apparatus. As a result, it was confirmed that the molecular weight was 848.16.
Synthetic example 1
[0161] Synthesis Example 1: Production of Compound Represented by Chemical Formula 3-1
[0162]
[0163] Potassium carbonate (0.04 mol) was added to the solution of INT (0.04 mol) and N-methylpyrrolidone (266.1 g) produced in Production Example 1, and the temperature was raised to 120°C. A liquid obtained by dissolving 4-fluorophenol (0.04 mol) in N-methylpyrrolidone (88.7 g) was added to the reaction solution at 120° C. for 2 hours. After maintaining the reaction at the same temperature for 1 hour, 4-chlorophenol (0.16 mol) and potassium carbonate (0.16 mol) were added, followed by stirring for 4 hours. The reaction solution was cooled to room temperature and discharged into 3 L of distilled water. The resulting red-purple precipitate was filtered under reduced pressure and washed with methanol water. The filtrate was redissolved in dichloromethane (MC), silica filtration was performed to remove impurities, and recrystallization was performed with MeOH to obtain the comp...
Synthetic example 2
[0165] Synthesis Example 2: Production of Compound Represented by Chemical Formula 3-3
[0166]
[0167]Potassium carbonate (0.04 mol) was added to the solution of INT (0.04 mol) and N-methylpyrrolidone (266.1 g) produced in Production Example 1, and the temperature was raised to 120°C. A liquid obtained by dissolving 2,4-bis(tert-butyl)phenol (0.04 mol) in N-methylpyrrolidone (88.7 g) was added to the reaction solution at 120° C. for 2 hours. After maintaining the reaction at the same temperature for 1 hour, 4-chlorophenol (0.16 mol) and potassium carbonate (0.16 mol) were added, followed by stirring for 4 hours. The reaction liquid was cooled to room temperature and discharged into 3 L of distilled water. The resulting red-purple precipitate was filtered under reduced pressure and washed with methanol water. The filtrate was redissolved in dichloromethane (MC), silica filtration was performed to remove impurities, and recrystallization was performed with MeOH to obtain ...
PUM
Property | Measurement | Unit |
---|---|---|
acid value | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com