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Method for measuring and calculating magnetic field induced phase transition temperature shift in variable magnetic martensite phase change Heusler alloy

A technology of martensitic transformation and measurement method, which is used in measurement devices, testing metals, and material analysis by electromagnetic means, etc., can solve the problems of complex calculation and many test data, and achieve simple calculation methods, reliable results, and test results. The effect of less data

Active Publication Date: 2018-08-14
CHINA THREE GORGES UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

This method requires a lot of test data and complex calculations

Method used

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  • Method for measuring and calculating magnetic field induced phase transition temperature shift in variable magnetic martensite phase change Heusler alloy
  • Method for measuring and calculating magnetic field induced phase transition temperature shift in variable magnetic martensite phase change Heusler alloy
  • Method for measuring and calculating magnetic field induced phase transition temperature shift in variable magnetic martensite phase change Heusler alloy

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Embodiment 1

[0027] 1. Put the sample to be tested into the vibrating sample magnetometer and evacuate to 4×10 3 Pa; load -3T magnetic field, and wait for the magnetic field to stabilize;

[0028] 2. Under the stable -3T magnetic field in the above steps, set the test temperature, set the magnetic field to sweep the field continuously from -3T to 3T, and test the curve of the resistance R of the sample changing with the magnetic field;

[0029] 3. Change the test temperature and repeat the test process of step 2, wherein the selection of test temperature points should cover the entire process of martensitic transformation;

[0030] 4. Measure the resistance temperature curve of the sample, and the temperature range covers the above measurement temperature points;

[0031] 5. According to the R-H curves at various temperatures obtained in the above step 3, analyze and calculate the magnitude of the temperature shift of the magnetically induced phase transition. Since the R-H curves near th...

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Abstract

The invention discloses a method for measuring and calculating the magnetic field induced phase transition temperature shift in a variable magnetic martensite phase change Heusler alloy. The method comprises the following steps: 1) placing a sample in a vibrating sample magnetometer, and vacuumizing the vibrating sample magnetometer; 2) loading the vibrating sample magnetometer into the magnetic field HM of the magnetic field induced martensite phase change size, and waiting for the magnetic field to be stable; 3) setting a test temperature in the magnetic field determined in step 2), settingcontinuous field sweep under the magnetic field from -HM to 0 and from 0 to HM, and testing the R-H curve of the resistance R of the sample with the change of the magnetic filed; 4) changing the testtemperature under the magnetic field determined in the step 2), and repeating the test process in step 3); and 5) calculating the size of the magnetic field induced phase transition temperature shiftat different temperatures according to the R-H curves at all temperatures, obtained in step 4). The macroscopic resistance change caused by the different characteristics of the magnetic transport property in every phase change stage during phase change is used to analyze and calculate the phase change temperature shift; and the method has the advantages of few required test data, simple calculation process and reliable result.

Description

technical field [0001] The invention belongs to the field of material physics, and in particular relates to a method for measuring and calculating the magnetic field-induced phase transition temperature shift in the magnetic field martensitic phase transition Hassler alloy. Background technique [0002] Magnetic field-induced phase transformation means that under the action of an external magnetic field, the alloy transforms from a high-symmetry cubic austenite phase to a low-symmetry martensite phase, resulting in a structural change with displacement and no diffusion. The driving force is the parent phase Zeeman energy difference between austenite and martensite phases. When the magnitude of the applied magnetic field is changed, the phase transition temperature of the alloy will move accordingly. In previous studies, there are two methods to determine the temperature shift of magnetically induced phase transition. One is to read the data from the test results of the magn...

Claims

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Application Information

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IPC IPC(8): G01N27/04G01N33/20
CPCG01N27/041G01N33/20
Inventor 潘礼庆许云丽杨栋超陈澄代智文易立志朴红光
Owner CHINA THREE GORGES UNIV
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