A high-performance zinc oxide varistor dielectric material and its preparation method
A varistor, dielectric material technology, applied in varistors, overvoltage protection resistors, etc., can solve the problems of small nonlinear coefficient and weak pulse shock resistance, and achieve high potential gradient, pulse shock resistance, etc. The effect of strong acceptability and simple preparation process
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Embodiment 1
[0027]First, synthesize Licrsi with solid phase method2O6(LA2 / 3ND1 / 3ALO3.
[0028]Licrsi2O6Using the following process preparation: Press 0.5: 0.5: 2 Molarby with Li2CO3, Cr2O3SiO2, Then pair Li2CO3, Cr2O3SiO2Grinding and mixing uniform; then li2CO3, Cr2O3SiO2The mixture was placed in an alumina crucible, and 120 minutes at 1180 ° C for 120 minutes to obtain Licrsi.2O6. Get Licrsi2O6After cooling, it is grinded and over 200 mesh sieves, spare.
[0029](La2 / 3ND1 / 3ALO3Preparation as follows: Press 1 / 3: 1 / 6: 1 / 2 of the molar ratio LA2O3ND2O3Alone2O3, Then pair LA2O3ND2O3Alone2O3Carry-up and mix evenly; then LA2O3ND2O3Alone2O3The mixture is placed in an alumina crucible, which is charged 120 minutes at 1220 ° C, resulting in (LA2 / 3ND1 / 3ALO3. Law2 / 3ND1 / 3ALO3After cooling, it is grinded and over 200 mesh sieves, spare.
[0030]Then, high-performance zinc oxide pressure sensitive resistor dielectric materials are prepared as follows:
[0031](1) Equipped with ZnO, SB2O3, CO2O3, BI2O3Ni2O3, Cr2O3, LICR...
Embodiment 2
[0044]First, synthesize Licrsi with solid phase method2O6(LA2 / 3ND1 / 3ALO3.
[0045]Licrsi2O6Using the following process preparation: Press 0.5: 0.5: 2 Molarby with Li2CO3, Cr2O3SiO2, Then pair Li2CO3, Cr2O3SiO2Grinding and mixing uniform; then li2CO3, Cr2O3SiO2The mixture is placed in an alumina crucible, and 120 minutes at 1150 ° C for 120 minutes to obtain Licrsi.2O6. Get Licrsi2O6After cooling, it is grinded and over 200 mesh sieves, spare.
[0046](La2 / 3ND1 / 3ALO3Preparation as follows: Press 1 / 3: 1 / 6: 1 / 2 of the molar ratio LA2O3ND2O3Alone2O3, Then pair LA2O3ND2O3Alone2O3Carry-up and mix evenly; then LA2O3ND2O3Alone2O3The mixture is placed in an alumina crucible, which is charged 120 minutes at 1200 ° C, resulting in (LA2 / 3ND1 / 3ALO3. Law2 / 3ND1 / 3ALO3After cooling, it is grinded and over 200 mesh sieves, spare.
[0047]Then, high-performance zinc oxide pressure sensitive resistor dielectric materials are prepared as follows:
[0048](1) Equipped with ZnO, SB2O3, CO2O3, BI2O3Ni2O3, Cr2O3, LICRS...
Embodiment 3
[0061]First, synthesize Licrsi with solid phase method2O6(LA2 / 3ND1 / 3ALO3.
[0062]Licrsi2O6Using the following process preparation: Press 0.5: 0.5: 2 Molarby with Li2CO3, Cr2O3SiO2, Then pair Li2CO3, Cr2O3SiO2Grinding and mixing uniform; then li2CO3, Cr2O3SiO2The mixture was placed in an alumina crucible, and 120 minutes were held at 1200 ° C to obtain Licrsi.2O6. Get Licrsi2O6After cooling, it is grinded and over 200 mesh sieves, spare.
[0063](La2 / 3ND1 / 3ALO3Preparation as follows: Press 1 / 3: 1 / 6: 1 / 2 of the molar ratio LA2O3ND2O3Alone2O3, Then pair LA2O3ND2O3Alone2O3Carry-up and mix evenly; then LA2O3ND2O3Alone2O3The mixture is placed in an alumina crucible, which is charged 120 minutes at 1250 ° C, resulting in (LA2 / 3ND1 / 3ALO3. Law2 / 3ND1 / 3ALO3After cooling, it is grinded and over 200 mesh sieves, spare.
[0064]Then, high-performance zinc oxide pressure sensitive resistor dielectric materials are prepared as follows:
[0065](1) Equipped with ZnO, SB2O3, CO2O3, BI2O3Ni2O3, Cr2O3, LICRSI2O6,...
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