A kind of high and low temperature resistant sleeve grouting material and preparation method thereof
A sleeve grouting, high and low temperature resistant technology, applied in the field of construction engineering
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preparation Embodiment 1
[0055] (1) Take 10.0kg tetramethyldivinyldisiloxane and 50kg octamethylcyclotetrasiloxane (D4) and place them in the reaction kettle, start the stirrer, add 3.0kg concentrated sulfuric acid as catalyst at the same time, heat up to 60°C, keep stirring under normal pressure for 6 hours, then lower to below 50°C to remove the filter agent, remove low molecular weight at 120-160°C for 5-8 hours at a pressure below 133Kpa, and obtain the intermediate vinyl-terminated polysilicon Oxygen, low molecular weight can be reused.
[0056] (2) After the above (1) reaction is completed, add 40kg rosin and 0.08kg hydroquinone catalyst, heat up to 200°C for Diels-Alder addition reaction, and after 6 hours of reaction, vacuumize to 3mmHg to remove the low boiling point impurities, the product was cooled to room temperature to obtain the rosin-modified silicone resin.
[0057] Water reducer preparation example 1
[0058] 1. Base material preparation
[0059] 30 kg of deionized water, 60 kg of...
preparation Embodiment 2
[0067] Other steps are the same as in Example 1, except that 2 kg of rosin-modified silicone resin is not added to the base material, but 3 kg of acrylic acid is added, and 3 kg of acrylic acid is not added in the dropping material A, but 2 kg of rosin-modified silicone resin is added. Silicone resin.
preparation Embodiment 3
[0069] Other conditions were the same as in Example 1, except that the amount of rosin-modified silicone resin added was 0.4 kg. Water reducer preparation example 4
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