A Vacuum Grading Gas Quenching Method for Thin-walled D6ac Ultra-High Strength Steel Shell

A technology of ultra-high-strength steel and thin-walled shells, which is applied in the field of quenching, can solve the problems of high dimensional accuracy and mechanical properties of the shell, affecting the dimensional accuracy and stability of the shell, reducing thermal stress and tissue stress, etc., to achieve Improve comprehensive mechanical properties, improve service performance, and reduce thermal stress

Active Publication Date: 2019-12-31
西安长峰机电研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Solid rocket motor casings and booster casings are thin-walled long tubes. After heat treatment, the requirements for dimensional accuracy and mechanical properties of the casing are high. After conventional heat treatment, large thermal stress and tissue stress are generated. These stresses lead to thin Large deformation of the wall shell or micro cracks appear, which affects the dimensional accuracy and stability of the shell
However, when using austenitic alloys for staged cooling and quenching, the temperature cannot be automatically adjusted when the austenite alloys are kept warm, and the operation is difficult. Moreover, the graded quenching process can only classify the austenite alloys, and cannot change the transformation from high temperature to pearlite. and martensite stage transformation, it is impossible to reduce thermal stress and structural stress in stages, and when the thin-walled shell is cooled in the air atmosphere, the temperature is not uniform
At the same time, there is a problem of decarburization when the thin-walled shell is heated in the air atmosphere, which affects the mechanical properties of the material
In addition, the pollution caused by oil quenching is large, which cannot meet the requirements of green environmental protection

Method used

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  • A Vacuum Grading Gas Quenching Method for Thin-walled D6ac Ultra-High Strength Steel Shell

Examples

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Effect test

Embodiment 1

[0035] A vacuum classification gas quenching method for D6AC ultra-high strength steel thin-walled shells described in this embodiment is specifically carried out according to the following steps: According to the content of the invention, the D6AC ultra-high strength steel is divided into two steps at a temperature of 6.7×10 -2 Heat to 900°C under Pa vacuum, keep it warm for 90min, cool to 780°C with 2bar high-purity nitrogen at a cooling rate of 15°C / min; Cool at a cooling rate of 520°C; after cooling, cool to 320°C at a cooling rate of 180°C / min; then cool from 320°C to below 50°C at a cooling rate of 5°C / min, and then leave the furnace for air cooling. After gas quenching, protect it with high-purity nitrogen gas, keep it at 550°C±10°C for 120min±10min, and then air cool it out of the furnace.

[0036] Example 1 After treatment, the tensile strength of D6AC ultra-high-strength steel matrix samples is between 1610MPa and 1640MPa, and the elongation after fracture is between...

Embodiment 2

[0038] A vacuum classification gas quenching method for D6AC ultra-high strength steel thin-walled shells described in this embodiment is specifically carried out according to the following steps: According to the content of the invention, the D6AC ultra-high strength steel is divided into two steps at a temperature of 6.7×10 -2 Heat to 900°C under Pa vacuum, keep it warm for 90min, cool to 780°C with 2bar high-purity nitrogen at a cooling rate of 15°C / min; Cool to 520°C at a cooling rate of 5°C / min; cool to 290°C at a cooling rate of 180°C / min after the heat preservation is over; cool from 290°C to below 50°C at a cooling rate of 5°C / min, and leave the oven for air cooling. After gas quenching, protect it with high-purity nitrogen gas, keep it at 550°C±10°C for 120min±10min, and then air cool it out of the furnace.

[0039] Example 2 The tensile strength of the D6AC ultra-high-strength steel matrix sample after treatment is between 1650MPa and 1660MPa, and the elongation afte...

Embodiment 3

[0041] A vacuum classification gas quenching method for D6AC ultra-high strength steel thin-walled shells described in this embodiment is specifically carried out according to the following steps: According to the content of the invention, the D6AC ultra-high strength steel is divided into two steps at a temperature of 6.7×10 -2Heat to 900°C under Pa vacuum, keep it warm for 90min, cool to 750°C with 2bar high-purity nitrogen at a cooling rate of 25°C / min; Cool at a cooling rate of 520°C; after cooling, cool to 320°C at a cooling rate of 300°C / min; cool from 320°C to below 50°C at a cooling rate of 8°C / min, and leave the furnace for air cooling. After gas quenching, protect it with high-purity nitrogen gas, keep it at 550°C±10°C for 120min±10min, and then air cool it out of the furnace.

[0042] Example 3 After treatment, the tensile strength of the D6AC ultra-high-strength steel matrix sample is between 1610MPa and 1640MPa, and the elongation after fracture is between 14.0% a...

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Abstract

The invention provides a vacuum step gas quenching method of a D6AC ultra-high strength steel thin-walled shell. The vacuum step gas quenching method of the D6AC ultra-high strength steel thin-walledshell comprises the steps of heating D6AC ultra-high strength steel to 900 degrees centigrade under a vacuum degree of 6.7x10<-2> Pa in two steps; cooling the D6AC ultra-high strength steel to 50 degrees centigrade under the atmosphere of 2 bar high-purity nitrogen in four steps; and discharging the D6AC ultra-high strength steel out of a furnace to be cooled by air. According to the vacuum step gas quenching method of the D6AC ultra-high strength steel thin-walled shell, by using a vacuum step gas quenching method, decarburization in heat treatment can be prevented, the mechanical performancecan be improved, deformation can be reduced, and meanwhile, the high-purity nitrogen is adopted to replace quenching oil, and the high-purity nitrogen is extracted from the air, and therefore, the production of the high-purity nitrogen is convenient, and the high-purity nitrogen is clean and pollution-free.

Description

technical field [0001] The invention relates to a quenching method. Background technique [0002] After quenching and tempering, the microstructure of D6AC ultra-high-strength steel is sorbite. It has high yield ratio, good ductility and notch toughness. It can still maintain high strength at high temperatures. It is mainly used in solid rocket motor casings and booster housing, etc. Solid rocket motor casings and booster casings are thin-walled long tubes. After heat treatment, the requirements for dimensional accuracy and mechanical properties of the casing are high. After conventional heat treatment, large thermal stress and tissue stress are generated. These stresses lead to thin The wall shell is deformed greatly or micro-cracks appear, which affects the dimensional accuracy and stability of the shell. However, when using austenitic alloys for staged cooling and quenching, the temperature cannot be automatically adjusted when the austenite alloys are kept warm, and th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21D1/613C21D1/19C21D1/773C21D6/00C21D9/00
CPCC21D1/19C21D1/613C21D1/773C21D6/00C21D9/0068
Inventor 李亚红杨立合王建国郑淑丽
Owner 西安长峰机电研究所
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