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96results about How to "Will not generate" patented technology

Preparation method and electroplating method of normal-temperature environment-friendly sulfate trivalent chromium electroplating liquid

The invention provides a preparation method and an electroplating method of normal-temperature environment-friendly sulfate trivalent chromium electroplating liquid, which relates to electroplating liquid and electroplating technology. The invention solves the problems of poor stability of the traditional trivalent chromium electroplating liquid, low precipitating and depositing rate of harmful gas in an electroplating process, more components of the electroplating liquid, sensitivity for impurities, poor corrosion resistance of an electroplating layer, and the like. The normal-temperature environment-friendly sulfate trivalent chromium electroplating liquid mainly comprises the following components of main salt, a complexation stabilizing agent, a combined additive, a buffering agent and a conducting salt. The electroplating liquid can work at normal temperature, thereby saving energy resources and having simple technology and high deposition rate, wherein the deposition rate can reach above 0.22micron.min<-1> under 6A / dm<2>. An anode of the invention is a Ti-based rare-metal tantalum-iridium-titanium anode, the anode oxygen-evolution overpotential is low, and harmful hexavalent chrome can not be generated. The normal-temperature environment-friendly sulfate trivalent chromium electroplating liquid has good corrosion resistance and high stability.
Owner:HARBIN INST OF TECH

Reduction method for a Fischer-Tropsch synthesis iron-based catalyst

The present invention relates to the field of Fischer-Tropsch synthesis iron-based catalyst reduction, and discloses a reduction method for a Fischer-Tropsch synthesis iron-based catalyst. The reduction method comprises: in the presence of a reducing gas, carrying out programmed heating reduction on Fischer-Tropsch synthesis iron-based catalyst particles in a fixed fluidized bed reactor, wherein the programmed heating reduction comprises that the heating rate is 10-20 DEG C / h and constant temperature treatment is performed for 2-8 h at a temperature of 120 DEG C when the temperature is from room temperature to 120 DEG C, the heating rate is 5-10 DEG C / h and constant temperature treatment is performed for 3-10 h at a temperature of 220-230 DEG C when the temperature is from 120 DEG C to (220-230) DEG C, and the heating rate is 3-5 DEG C / h and constant temperature treatment is performed for 10-30 h at a temperature of 260-280 DEG C when the temperature is from (220-230) DEG C to (260-280) DEG C. With the reduction method of the present invention, the Fischer-Tropsch synthesis iron-based catalyst can be smoothly subjected to the reduction reaction so as to reduce the influence on the water and the catalyst strength, and with the application of the reduced catalyst in the Fischer-Tropsch synthesis, the advantages of no breaking, high catalyst activity, low CO2 selectivity and low low-carbon hydrocarbon selectivity can be provided.
Owner:CHNA ENERGY INVESTMENT CORP LTD +1

Coaxial heating chamber and electronic cigarette device with coaxial heating chamber

PendingCN110141002AHeating evenlyThere will be no local high temperatureTobacco devicesElectrical conductorElectronic cigarette
The invention discloses a coaxial heating chamber and an electronic cigarette device with the coaxial heating chamber. The electronic cigarette device with the coaxial heating chamber includes a coaxial heating chamber which is formed by the fact that an outer conductor chamber is regarded as a chamber, and an inner conductor column which is regarded as a column and inserts from one end of the outer conductor chamber into the outer conductor chamber; and a microwave source from one end of the inner conductor column inserted into the outer conductor chamber into the coaxial heating chamber to conduct microwave transmission to achieve the heating of microwave to a tobacco. A coaxial transmitter and the coaxial heating chamber are used, microwaves with the frequency of 915MHz and 2.45GHz canbe transmitted in the coaxial transmitter and the coaxial heating chamber, and therefore, a relatively mature solid-state microwave device can be used, especially 915MHz electrical conversion efficiency is higher; the size of the device can be effectively controlled; and due to the fact that the microwave has no temperature, through high frequency alternating electric field, polar molecules in thetobacco is made directly to move and heat, tobacco overall temperature is controlled in 200~300 DEG C, local high temperature does not exist, higher temperature does not exist in the overall coaxialheating chamber and the tobacco, cracking does not occur, and aldehyde or other harmful substances cannot be produced.
Owner:YUNNAN TOBACCO BIOLOGICAL TECH CO LTD +1

Magnesium/steel layered composite material and preparation method thereof

The invention relates to a magnesium/steel layered composite material and a preparation method thereof, belonging to the field of metal layered composite materials. The magnesium/steel layered composite material of the present invention is formed by interfacial metallurgical bonding of magnesium material and steel material, without an intermediate layer between the magnesium material and the steelmaterial, and is prepared by the steps of mechanical grinding surface treatment, alternating lamination and combination to form composite blanks, wrapping the composite blanks with metal sleeve and performing vacuum treatment, heating, hot rolling, diffusion heat treatment after removing the metal sleeve, and the like. The invention has the advantages that the magnesium/steel layered composite material has both excellent mechanical properties and vibration damping properties, can be used at the working temperature of 200-600 DEG C for a long time without solid solution or intermetallic compound at that interface between magnesium and steel, the interfacial bonding strength is stable or even gradually increased in the working temperature range, and the magnesium/steel layered composite billet need not be heated in vacuum or inert gas atmosphere, so the operation is convenient, the requirement for equipment is low, the price of required equipment is cheap, and the production cost is low, so the composite billet has universal popularization and application value.
Owner:UNIV OF SCI & TECH BEIJING

Method for preparing cobaltosic oxide nanorod by using microemulsion

InactiveCN102115213AExperimental raw materials are cheapAvoid pollutionCatalyst carriersNanotechnologyChemistrySolution composition
The invention discloses a method for preparing a cobaltosic oxide nanorod by using microemulsion. A double microemulsion system and a single emulsion system are provided, wherein the double microemulsion system consists of a microemulsion I and a microemulsion II; each of the microemulsion I and the microemulsion II consists of CTAB (Cetyltrimethyl Ammonium Bromide) serving as a surfactant, normal butanol serving as a cosurfactant, oil phase cyclohexane and a water phase; the mass ratio of the oil phase to the water phase is 1:20-20:1; and in the microemulsion I, the water phase is a CoCl2 aqueous solution; in the microemulsion II, the water phase is an H2C2O4 solution. Polyethylene glycol serving as a dispersant is added into the system, wherein the polyethylene glycol accounts for 10-80 percent by mass of the entire microemulsion system (the double microemulsions comprise the microemulsion I and the microemulsion II, the single microemulsion comprises the microemulsion I, and the double microemulsions and the single microemulsion do not comprise the polyethylene glycol). The single microemulsion system consists of the microemulsion I and the H2C2O4 aqueous solution, and the composition of the microemulsion I is the same as that of the microemulsion I in the double microemulsions. By adopting the method, the diameter of the obtained nanorod is between 70 nanometers and 150 nanometers, and the length is between 1 mu m and 3 mu m.
Owner:BEIJING UNIV OF CHEM TECH +1

Temperature control method for slurry bed reactor, design method and application thereof

The invention provides a temperature control method for a slurry bed reactor, a design method and the application thereof. The method comprises the step of injecting a coolant in pipes in front of the inlets of a reactors at all levels. The pipes are connected with at least one coolant pipeline to realize the temperature control. The coolant is composed of cold hydrogen and cold oil. According to the method, the method can be applied to reactors during the heavy oil hydrodesulfurization process, the direct coal liquefaction process and the oil-coal mixing process. Through adjusting the number of coolant pipelines and the flow of the coolant, the reaction temperature of the reactor can be controlled. The method is easy to realize during the project implementation process, and facilitates the automatic control. Meanwhile, the operation stability of the reactor is improved. Cold hydrogen and cold oil are necessary raw materials for the reaction, and the forestage reaction heat of the reactor is fully utilized. Therefore, the efficient utilization of heat is realized. The method is especially suitable for second-stage reactors and third-stage reactors. For first-stage reactors, the temperature control effect can still be realized through respectively heating two ways of hydrogen and then mixing up the two ways of hydrogen.
Owner:CATECH TECH

Harmless treatment method and system of lithium metal waste residue

The invention discloses a harmless treatment method and system of lithium metal waste residue. The harmless treatment method of the lithium metal waste residue comprises the following steps: putting the lithium metal waste residue in a sealed heating chamber and completely replacing gas in the heating chamber with protective gas which does not react with lithium; heating the lithium metal waste residue to a first temperature, disturbing the lithium metal waste residue, and vacuumizing the heating chamber in order to achieve oil removal treatment; after finishing the oil removal treatment, heating the lithium metal waste residue to a second temperature and disturbing the lithium metal waste residue in order to cause the lithium metal to melt and aggregate into lithium metal liquid and layerthe lithium metal liquid with solid impurities; and enabling the lithium metal liquid to flow out from the heating chamber after passing through a filter net placed in the heating chamber in order tointercept the solid impurities by the filter net. The harmless treatment method has no chemical reaction and no contact with air during treating the lithium metal waste residue, eliminates potentialsafety hazards, can directly, rapidly and effectively recover the lithium metal from the lithium metal waste residue, and has simple process and high economic benefit.
Owner:天齐锂业(江苏)有限公司

Agent for removing heavy metal ions from water and preparation method of agent

The invention relates to sewage treatment agents, in particular to a preparation method and use of an agent for removing heavy metal ions from water. According to the technical scheme, the agent comprises the following raw materials in part by weight: 2 parts of natural weathered coal and 1 part of 30-50% of a sodium hydroxide solution. The preparation method comprises the following steps: (1) grinding the natural weathered coal; (2) carrying out a reaction between the ground weathered coal and the sodium hydroxide solution at the temperature of 60-80 DEG C for 5-10 h; (3) clarifying the reaction solution, sucking supernatant, and filtrating the supernatant for later use; (4) heating the filtrated supernatant which is protected by nitrogen to 50-60 DEG C in a reaction vessel to realize a polymerization reaction for 2-3 h; (5) taking out the polymer for drying. The preparation method has the advantages as follows: (1) adjusting the pH value in water is avoided when the agent is in use, and the agent can be directly put in water containing the heavy metal ions; (2) no toxic and harmful gas is generated after a coagulation reaction; (3) the weathered coal taken as a raw material is cheap, so that the preparation method provided by the invention is suitable for popularization and application.
Owner:中关村科技租赁股份有限公司

Magnesium alloy oxidation coloring method and product thereof

The invention discloses a magnesium alloy oxidation coloring method and a product thereof. The magnesium alloy oxidation coloring method comprises the steps: (1) degreasing magnesium alloy; (2) carrying out acid pickling on the degreased magnesium alloy; (3) carrying out surface conditioning on the magnesium alloy subjected to acid pickling; (4) baking the magnesium alloy subjected to surface conditioning; (5) feeding the baked magnesium alloy; (6) carrying out electrolytic coloring on the fed magnesium alloy; and (7) baking the magnesium alloy subjected to electrolytic coloring. The product is produced by using the magnesium alloy oxidation coloring method. The magnesium alloy oxidation coloring is combined with formation pretreatment and is simple and convenient in operation process and good in effect, the defect of single color for surface treatment on magnesium alloy is overcome, the range of a requirement for the quality of the surface of a material is relatively wide, the corrosion resistance and wear resistance of the magnesium alloy are greatly improved by the surface appearance of a coloring sample, the coloring process is relatively environment-friendly, a great number of harmful substances cannot be produced in an oxidation reaction process, and therefore, the magnesium alloy oxidation coloring method is suitable for factory quantified production.
Owner:KUNSHAN HANDING PRECISION METAL CO LTD
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