The invention provides a synthesis process of ultrafine-grade
diamond. The synthesis process comprises the steps: after mixing a
graphite powder and an Fe-based
alloy catalyst
powder according to the weight ratio of 8:5-7, carrying out isostatic pressing treatment and vacuum treatment, then carrying out press forming in a four-column pressing
machine, followed by putting the column core into
a diamond synthetic block, next putting the
diamond synthetic block into a six-side jacking press
machine, and synthesizing, wherein the actual synthesis pressure is 6.1-6.6 GPa, the synthesis temperature is 1000-1100 DEG C, and the actual synthesis pressure and the synthesis temperature are completed respectively by adopting a control
pressure curve and a power curve. The synthesized
diamond with micron-sized fine particles has the characteristics of large
nucleation amount, short
growth time and the like; the product meets national artificial diamond standards, has the advantages of consistent
crystal form, integral
crystal faces, less impurities and
high heat flush value, has the particle
granularity with peak values of 270 / 325 and 325 / 400, allows the
single crystal ratio to reach 70-80%, and can effectively meet the fields of high-end
abrasive tools and the like having extremely high requirements on the particle
fineness.