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a ti 3 alc 2 Method for preparing ceramic-bonded diamond drilling tool bit

A ceramic bond, diamond tip technology, used in metal processing equipment, manufacturing tools, grinding/polishing equipment, etc., to achieve the effect of good chemical bonding, low density, and shortened process flow

Active Publication Date: 2021-10-12
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, Ti is prepared by microwave-enhanced self-propagating reaction. 3 AlC 2 Cermets, especially in the preparation of Ti 3 AlC 2 The field of bonded diamond segment has not been reported yet

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A kind of Ti 3 AlC 2 The preparation method of base vitrified bond diamond drilling tool cutter head, select Ti powder, Al powder and C powder that particle size is 300 meshes, take by weighing according to the ratio of Ti: Al: C=3: 1: 2 according to molar ratio, in ball mill Mix well in the medium for 5 hours to obtain a uniformly mixed powder; add diamond particles with a volume percentage of 10% to the obtained powder, and mix for 1 hour to obtain a formula; fill the formula into a cold pressing mold, and use a cold press to form it. The pressure was controlled at 10 MPa to obtain a cold-pressed compact with a size of 55×10×10 mm; the obtained cold-pressed compact was put into a microwave pressureless sintering furnace protected by argon, and 2450MHz microwave energy was used as the heat source, and the microwave power was 3kW. According to the time of 6s, the cold compact is ignited and a self-propagating sintering reaction occurs, and the microwave is maintained f...

Embodiment 2

[0024] A kind of Ti 3 AlC 2 The preparation method of base vitrified bond diamond drilling tool cutter head, select Ti powder, Al powder and C powder that particle size is 300 meshes, according to molar ratio be Ti: Al: C=2.9: 1: 2.1 ratio by weighing, in ball mill Mix well in the medium for 6 hours to obtain a uniformly mixed powder; add diamond particles with a volume percentage of 20% to the obtained powder, and mix for 2 hours to obtain a formula; fill the formula into a cold pressing mold, and use a cold press to form it. The pressure was controlled at 20MPa to obtain a cold-pressed compact with a size of 55×10×10 mm; the obtained cold-pressed compact was put into an argon-protected microwave pressureless sintering furnace, using 2450MHz microwave energy as the heat source, and the microwave power was 4kW. According to the time of 10s, the cold compact is ignited and a self-propagating sintering reaction occurs, and the microwave is maintained for 50s to obtain Ti 3 AlC...

Embodiment 3

[0026] A kind of Ti 3 AlC 2 The preparation method of the base vitrified bond diamond drilling tool cutter head, select Ti powder, Al powder and C powder with particle size of 300 mesh, according to the ratio of Ti: Al: C=3.1: 1: 1.9 according to the molar ratio, take by weighing in the ball mill Mix well in the medium for 7 hours to obtain a uniformly mixed powder; add diamond particles with a volume percentage of 30% to the obtained powder, and mix for 3 hours to obtain a formula; fill the formula into a cold press mold, and use a cold press to form it. The pressure was controlled at 30MPa to obtain a cold-pressed compact with a size of 55×10×10 mm; the obtained cold-pressed compact was put into a microwave pressureless sintering furnace protected by argon gas, and 2450MHz microwave energy was used as the heat source, and the microwave power was 5kW. According to the time of 15s, the cold compact is ignited and a self-propagating sintering reaction occurs, and the microwave...

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Abstract

The present invention relates to a kind of Ti 3 AlC 2 The invention discloses a method for preparing a ceramic bonded diamond drilling tool head, which belongs to the technical field of superhard material tool preparation. The method of the present invention: use elemental Ti powder, Al powder, and C powder as binder raw materials and diamond abrasives to be weighed and mixed according to a certain proportion, dry, and cold-press to form a billet; place the compact in an argon-protected reactor, and use Preparation of Ti by Microwave as Induced Heat Source Ignition and Self-propagating Reaction Sintering 3 AlC 2 Ceramic based diamond drilled tool bit. The invention uses microwave ignition to strengthen the self-propagating process, which is beneficial to the rapid migration of liquid phase elements in the sintered body, accelerates the escape of gas inside the sintered body during the densification process, and makes the sintered structure of the sample uniform, which can significantly increase the Ti 3 AlC 2 Based on the production efficiency of diamond tool cutter heads, diamond tool products with excellent comprehensive mechanical properties are obtained.

Description

technical field [0001] The present invention relates to a kind of Ti 3 AlC 2 The invention discloses a method for preparing a ceramic-bonding agent diamond drilling tool head, which belongs to the field of superhard material tool preparation. Background technique [0002] Diamond tools are widely used in the field of drilling due to their advantages of high efficiency, high precision, high strength and low environmental pollution. The composite material of the working layer usually uses metal, ceramics and resin as binders, which are mixed with diamond abrasives. It is sintered at high temperature, and ceramic materials are the main category for preparing diamond abrasive bond. [0003] At present, the commonly used ceramic-based binders mostly use oxides, glass or microcrystals as the main components. After adding a large amount of alkaline materials, they are sintered to obtain the binder. The thermal expansion coefficient between the matrix and the diamond is poorly mat...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/56C04B35/64B24D3/14B24D3/34B24D18/00
CPCB24D3/14B24D3/342B24D18/0009C04B35/56C04B35/64C04B2235/402C04B2235/404C04B2235/422C04B2235/96
Inventor 杨黎侯明郭胜惠彭金辉胡途叶小磊
Owner KUNMING UNIV OF SCI & TECH