Photonic crystal structure and Anti-forgery color conversion film comprising same
A photonic crystal, color conversion technology, applied in optics, optical components, chemical instruments and methods, etc., can solve the problems of high product cost, expensive, large RFID tags and so on
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preparation Embodiment A
[0342] Preparation Example A: Preparation of BPAA
[0343] After introducing 9.86 g of 4-aminobenzophenone, 15 mL of triethylamine, and 80 mL of dichloromethane into the 250 mL round bottom flask, the flask was placed in ice water. 4.06 mL of acryloyl chloride was added to the flask, and the mixture was stirred for 12 hours. After the reaction was complete, the solvent was removed and then dried in a vacuum oven to obtain N-(4-benzoylphenyl)acrylamide as a yellow solid.
preparation Embodiment B
[0344] Preparation Example B: Preparation of BPA
[0345] After introducing 10 g of 4-hydroxybenzophenone, 20 mL of triethylamine, and 120 mL of dichloromethane into a 250 mL round bottom flask, the flask was placed in ice water. 4.92 mL of acryloyl chloride was added to the flask, and the mixture was stirred for 12 hours. After the reaction was complete, the solvent was removed, followed by drying in a vacuum oven to obtain 4-acryloyloxybenzophenone as a yellow solid.
preparation Embodiment C
[0346] Preparative Example C: Preparation of FEAA
[0347]After introducing 10 g of 2-fluoroethylamine and 12 mL of triethylamine into the round bottom flask, the flask was placed in ice water. 7.7 mL of acryloyl chloride was slowly added dropwise into the flask with stirring. When all the solution was added, the mixture was stirred at room temperature for 12 hours. After the reaction was complete, the solvent was removed using a rotary evaporator to obtain pure N-(2-fluoroethyl)acrylamide as a yellow liquid.
[0348] Synthesis of Copolymer
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