Bi-component flexible compound epoxy resin adhesive
A technology of epoxy resin glue and epoxy resin, which is applied in the direction of epoxy resin glue, polymer adhesive additives, non-polymer adhesive additives, etc., can solve the problems that cannot be improved together, so as to avoid cracking failure, The effect of toughness improvement and toughness enhancement
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[0029] Example 1
[0030] After mixing graphene oxide and isocyanate in a mass ratio of 1:5, heating and stirring to react, filtering, washing and vacuum drying, pretreated graphene oxide is obtained; silicon dioxide and 12% hydrochloric acid by mass Mix at a ratio of 1:15, stir and react for 4 hours at a temperature of 120°C and a speed of 400r / min, and then filter to obtain an activated silica blank. The activated silica blank is washed with deionized water until the washing solution is After neutralization, and after drying for 2h at a temperature of 100℃, and then calcining at a temperature of 300℃ for 2h, activated silica is obtained. The activated silica is combined with the silane coupling agent KH-550. The mass ratio of 1:3 was mixed in the flask, and 12 times the mass of activated silica was added to the flask. The reaction was stirred for 3 hours at a temperature of 85°C and a speed of 400r / min, and then at room temperature. After standing for 3 hours, filter to obtain...
Example Embodiment
[0031] Example 2
[0032] Mix silica and 12% hydrochloric acid with a mass ratio of 1:15. Under the conditions of a temperature of 120°C and a speed of 400r / min, the reaction is stirred for 4 hours, and then filtered to obtain an activated silica blank. After the activated silica blank is washed with deionized water until the washing solution is neutral, dried at a temperature of 100°C for 2 hours, and then calcined at a temperature of 300°C for 2 hours to obtain activated silica. Activated silica and silane coupling agent KH-550 were mixed in a flask at a mass ratio of 1:3, and 12 times the mass of activated silica was added to the flask with anhydrous ethanol at a temperature of 85°C and a rotation speed of 400r Stir and react for 3h under the condition of 1 / min, and then stand still at room temperature for 3h, and then filter to obtain the aminated silica blank. After the aminated silica blank is dried at a temperature of 80℃ for 3h, the amino group is obtained. Silica, which...
Example Embodiment
[0033] Example 3
[0034] Mix silica and 12% hydrochloric acid with a mass ratio of 1:15. Under the conditions of a temperature of 120°C and a speed of 400r / min, the reaction is stirred for 4 hours, and then filtered to obtain an activated silica blank. After the activated silica blank is washed with deionized water until the washing solution is neutral, dried at a temperature of 100°C for 2 hours, and then calcined at a temperature of 300°C for 2 hours to obtain activated silica. Activated silica and silane coupling agent KH-550 were mixed in a flask at a mass ratio of 1:3, and 12 times the mass of activated silica was added to the flask with anhydrous ethanol at a temperature of 85°C and a rotation speed of 400r Stir and react for 3h under the condition of 1 / min, and then stand still at room temperature for 3h, and then filter to obtain the aminated silica blank. After the aminated silica blank is dried at a temperature of 80℃ for 3h, the amino group is obtained. For silica, m...
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